C₁₂H₁₈

Base Information

• Chemical Name: C₁₂H₁₈
• CAS No.: 1453804-00-6
• Molecular Formula: C₁₂H₁₈
• Molecular Weight: 162.275
• Mol file: 1453804-00-6.mol

Synonyms:

Chemical Property of C₁₂H₁₈

Chemical Property:

Purity/Quality:

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Technology Process of C₁₂H₁₈

There total 1 articles about C₁₂H₁₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1-methyl-1,2-propadienyl)cyclohexane (59409-49-3) + tris-iso-propylsilyl acetylene (89343-06-6) → C12H18 (1453804-00-6) + C12H18 + C12H18

Guidance literature:

(1-methyl-1,2-propadienyl)cyclohexane; tris-iso-propylsilyl acetylene; With cobalt(II) acetate tetrahydrate; C₃₆H₃₈FeP₂; zinc; In dimethyl sulfoxide; at 80 ℃; for 3h; Inert atmosphere;

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h; Overall yield = 88 %; Overall yield = 56 mg; enantioselective reaction; Inert atmosphere;

DOI:10.1021/jo401604n

upstream raw materials:

(1-methyl-1,2-propadienyl)cyclohexane

tris-iso-propylsilyl acetylene