C₂₄H₂₇FN₄O₄S₂

Base Information

Chemical Name:C₂₄H₂₇FN₄O₄S₂
CAS No.:1410798-64-9
Molecular Formula:C₂₄H₂₇FN₄O₄S₂
Molecular Weight:518.633
Hs Code.:

C<sub>24</sub>H<sub>27</sub>FN<sub>4</sub>O<sub>4</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₂₄H₂₇FN₄O₄S₂

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Technology Process of C₂₄H₂₇FN₄O₄S₂

There total 6 articles about C₂₄H₂₇FN₄O₄S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1078627-28-7
1-methyl-cyclopropyl carbonochloridate

: C₁₉H₂₁FN₄O₂S₂

: 1410798-64-9
C₂₄H₂₇FN₄O₄S₂

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2014.07.020

Reference yield:

: 79099-07-3
N-tert-butyloxycarbonylpiperidin-4-one

: 1410798-64-9
C₂₄H₂₇FN₄O₄S₂

Guidance literature:: Multi-step reaction with 5 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 24 h

2: dimethyl sulfoxide / 60 °C

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,4-dioxane / 3 h / 110 °C / Sealed tube

4: hydrogenchloride / water; 1,4-dioxane / 2 h / 20 °C

5: triethylamine / dichloromethane / 1 h / 20 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; hydrogen; sodium carbonate; triethylamine; In 1,4-dioxane; methanol; dichloromethane; water; dimethyl sulfoxide; 3: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.07.020

Reference yield:

: 31169-27-4
7-bromo-4-chlorothieno[3,2-d]pyrimidine

: 1410798-64-9
C₂₄H₂₇FN₄O₄S₂

Guidance literature:: Multi-step reaction with 4 steps

1: dimethyl sulfoxide / 60 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / 1,4-dioxane / 3 h / 110 °C / Sealed tube

3: hydrogenchloride / water; 1,4-dioxane / 2 h / 20 °C

4: triethylamine / dichloromethane / 1 h / 20 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; triethylamine; In 1,4-dioxane; dichloromethane; water; dimethyl sulfoxide; 2: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.07.020