2-methyl-d3-2-phenylheptanoic acid

Base Information

Chemical Name:2-methyl-d3-2-phenylheptanoic acid
CAS No.:1534433-66-3
Molecular Formula:C₁₄H₂₀O₂
Molecular Weight:223.288
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methyl-d3-2-phenylheptanoic acid

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Technology Process of 2-methyl-d3-2-phenylheptanoic acid

There total 2 articles about 2-methyl-d3-2-phenylheptanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₁₉⁽²⁾H₃O₂

: 1534433-66-3
2-methyl-d3-2-phenylheptanoic acid

Guidance literature:: With water; sodium hydroxide; In methanol; at 100 ℃; for 24h;
DOI:10.1021/ja411715v

Reference yield:

: 1534433-67-4
methyl 2-phenylheptanoate

: 1534433-66-3
2-methyl-d3-2-phenylheptanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; diisopropylamine; lithium diisopropyl amide / hexane; tetrahydrofuran / 1 h / -78 °C

1.2: 5 h / -78 - 20 °C

2.1: sodium hydroxide; water / methanol / 24 h / 100 °C

With n-butyllithium; water; diisopropylamine; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane;
DOI:10.1021/ja411715v

Reference yield:

: 1534433-66-3
2-methyl-d3-2-phenylheptanoic acid

: C₁₄H₁₆⁽²⁾H₃ClO

Guidance literature:: With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; at 0 - 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ja411715v