N-{5-[4-(tert-butyldimethylsilanyloxy)-5-hydroxymethyl-2,5-dihydrofuran-2-yl]-1-methyl-4-oxo-1,2,3,4-tetrahydropyrimidin-2-yl}-2,2-dimethylpropionamide

Base Information

Chemical Name:N-{5-[4-(tert-butyldimethylsilanyloxy)-5-hydroxymethyl-2,5-dihydrofuran-2-yl]-1-methyl-4-oxo-1,2,3,4-tetrahydropyrimidin-2-yl}-2,2-dimethylpropionamide
CAS No.:1193570-05-6
Molecular Formula:C₃₁H₃₉N₃O₅Si
Molecular Weight:561.753
Hs Code.:

N-{5-[4-(tert-butyldimethylsilanyloxy)-5-hydroxymethyl-2,5-dihydrofuran-2-yl]-1-methyl-4-oxo-1,2,3,4-tetrahydropyrimidin-2-yl}-2,2-dimethylpropionamide

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Chemical Property of N-{5-[4-(tert-butyldimethylsilanyloxy)-5-hydroxymethyl-2,5-dihydrofuran-2-yl]-1-methyl-4-oxo-1,2,3,4-tetrahydropyrimidin-2-yl}-2,2-dimethylpropionamide

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Technology Process of N-{5-[4-(tert-butyldimethylsilanyloxy)-5-hydroxymethyl-2,5-dihydrofuran-2-yl]-1-methyl-4-oxo-1,2,3,4-tetrahydropyrimidin-2-yl}-2,2-dimethylpropionamide

There total 1 articles about N-{5-[4-(tert-butyldimethylsilanyloxy)-5-hydroxymethyl-2,5-dihydrofuran-2-yl]-1-methyl-4-oxo-1,2,3,4-tetrahydropyrimidin-2-yl}-2,2-dimethylpropionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1193570-03-4
5-iodo-1-methyl-2-pivaloylamino-4-pyrimidinone

: 130277-32-6
((2R,3S)-3-(tert-butyldiphenylsilyloxy)-2,3-dihydrofuran-2-yl)methanol

: 1263427-62-8
C₁₀H₁₅N₃O₂

: 1193570-05-6
N-{5-[4-(tert-butyldimethylsilanyloxy)-5-hydroxymethyl-2,5-dihydrofuran-2-yl]-1-methyl-4-oxo-1,2,3,4-tetrahydropyrimidin-2-yl}-2,2-dimethylpropionamide

Guidance literature:: With tributyl-amine; triphenyl-arsane; palladium diacetate; In N,N-dimethyl-formamide; at 60 ℃; for 72h; Inert atmosphere;
DOI:10.1080/15257770902946090