2-hydroxy-5-methoxyphenyl 2,4,6-trimethoxyphenylmethanone

Base Information

Chemical Name:2-hydroxy-5-methoxyphenyl 2,4,6-trimethoxyphenylmethanone
CAS No.:42832-64-4
Molecular Formula:C₁₇H₁₈O₆
Molecular Weight:318.326
Hs Code.:

Synonyms:

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Chemical Property of 2-hydroxy-5-methoxyphenyl 2,4,6-trimethoxyphenylmethanone

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Technology Process of 2-hydroxy-5-methoxyphenyl 2,4,6-trimethoxyphenylmethanone

There total 5 articles about 2-hydroxy-5-methoxyphenyl 2,4,6-trimethoxyphenylmethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 621-23-8
1,2,3-trimethoxybenzene

: 15198-09-1
2-hydroxy-5-methoxy-benzoyl chloride

: 42832-64-4
2-hydroxy-5-methoxyphenyl 2,4,6-trimethoxyphenylmethanone

Guidance literature:: 1,2,3-trimethoxybenzene; 2-hydroxy-5-methoxy-benzoyl chloride; With aluminum (III) chloride; In diethyl ether; at 90 ℃;

With hydrogenchloride; In water; at 70 ℃; for 0.5h;
DOI:10.1002/ardp.201100279

Reference yield:

: 77-78-1
dimethyl sulfate

: 2'-O-β-D-glucopyranosyl-2,4,5',6-tetrahydroxybenzophenone

: 42832-64-4
2-hydroxy-5-methoxyphenyl 2,4,6-trimethoxyphenylmethanone

Guidance literature:: dimethyl sulfate; 2'-O-β-D-glucopyranosyl-2,4,5',6-tetrahydroxybenzophenone; With potassium carbonate; In acetone;

With hydrogenchloride; In methanol; for 3h; Heating;
DOI:10.1016/S0031-9422(01)00194-7

Reference yield:

: 2785-98-0
2,5-dimethoxybenzoic acid

: 42832-64-4
2-hydroxy-5-methoxyphenyl 2,4,6-trimethoxyphenylmethanone

Guidance literature:: Multi-step reaction with 2 steps

1: oxalic acid dichloride / benzene / 1 h / Heating

2: AlCl₃ / diethyl ether / 28 h / Ambient temperature

With aluminium trichloride; oxalyl dichloride; In diethyl ether; benzene;
DOI:10.1002/ardp.19903230307