(4aR)-4a,5,6,7,8,8aα,9,9aα-Octahydro-3,4aβ,5β-trimethylnaphtho[2,3-b]furan-2(4H)-one

Base Information

Chemical Name:(4aR)-4a,5,6,7,8,8aα,9,9aα-Octahydro-3,4aβ,5β-trimethylnaphtho[2,3-b]furan-2(4H)-one
CAS No.:29395-64-0
Molecular Formula:C₁₅H₂₂O₂
Molecular Weight:234.338
Hs Code.:
Mol file:29395-64-0.mol

Synonyms:10a-Eremophil-7(11)-en-12-oic acid,8-hydroxy-, g-lactone,(-)- (8CI); Naphtho[2,3-b]furan-2(4H)-one,4a,5,6,7,8,8a,9,9a-octahydro-3,4a,5-trimethyl-, [4aR-(4aa,5a,8ab,9ab)]-; Ligularenolide, tetrahydro-;Tetrahydroligularenolide

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4aR)-4a,5,6,7,8,8aα,9,9aα-Octahydro-3,4aβ,5β-trimethylnaphtho[2,3-b]furan-2(4H)-one

Chemical Property:

PSA：26.30000
LogP:3.46460

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (4aR)-4a,5,6,7,8,8aα,9,9aα-Octahydro-3,4aβ,5β-trimethylnaphtho[2,3-b]furan-2(4H)-one

There total 20 articles about (4aR)-4a,5,6,7,8,8aα,9,9aα-Octahydro-3,4aβ,5β-trimethylnaphtho[2,3-b]furan-2(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: (Z)-cis-4β,5b-dimethyl-8-decalone-7-ylidene-N,N-diethylmethacrylcarboxamide

: 4871-90-3,22387-76-4,29395-64-0,33118-37-5,43206-20-8,70518-33-1
(+/-)-Eremophilenolid

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 3h; Ambient temperature;

Reference yield: 70.0%

: (+/-)-eremophiledinone

: 4871-90-3,22387-76-4,29395-64-0,33118-37-5,43206-20-8,70518-33-1
(+/-)-Eremophilenolid

Guidance literature:: (+/-)-eremophiledinone; With sodium tetrahydroborate; In methanol; at 20 ℃;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; benzene; Reflux;
DOI:10.1016/j.tetlet.2008.08.006

Reference yield:

: 20489-24-1
eremophil-1(10),7(11),8-trien-12,8-olide

: 29395-64-0
(-)tetrahydroligularenolide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 12h; Ambient temperature;
DOI:10.1016/0031-9422(93)85374-Z