N-benzyloxycarbonyl-O-methyl-L-α-aspartyl=>N^ω-nitro-L-arginyl=>L-valyl=>L-tyrosyl=>L-isoleucyl=>L-histidyl=>L-prolyl=>L-phenylalanine-methyl ester

Base Information

• Chemical Name: N-benzyloxycarbonyl-O-methyl-L-α-aspartyl=>N^ω-nitro-L-arginyl=>L-valyl=>L-tyrosyl=>L-isoleucyl=>L-histidyl=>L-prolyl=>L-phenylalanine-methyl ester
• CAS No.: 133103-10-3
• Molecular Formula: C₆₀H₈₀N₁₄O₁₆
• Molecular Weight: 1253.38

Synonyms:

Chemical Property of N-benzyloxycarbonyl-O-methyl-L-α-aspartyl=>N^ω-nitro-L-arginyl=>L-valyl=>L-tyrosyl=>L-isoleucyl=>L-histidyl=>L-prolyl=>L-phenylalanine-methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of N-benzyloxycarbonyl-O-methyl-L-α-aspartyl=>N^ω-nitro-L-arginyl=>L-valyl=>L-tyrosyl=>L-isoleucyl=>L-histidyl=>L-prolyl=>L-phenylalanine-methyl ester

There total 2 articles about N-benzyloxycarbonyl-O-methyl-L-α-aspartyl=>N^ω-nitro-L-arginyl=>L-valyl=>L-tyrosyl=>L-isoleucyl=>L-histidyl=>L-prolyl=>L-phenylalanine-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Nα-(N-benzyloxycarbonyl-O-methyl-L-α-aspartyl)-Nω-nitro-L-arginine → N-benzyloxycarbonyl-O-methyl-L-α-aspartyl=>Nω-nitro-L-arginyl=>L-valyl=>L-tyrosyl=>L-isoleucyl=>L-histidyl=>L-prolyl=>L-phenylalanine-methyl ester (133103-10-3)

Guidance literature:

aufeinanderfolgendes Behandeln mit Tributylamin und Chlorokohlensaeure-aethylester in Dioxan und mit L-valyl$>L-tyrosyl$>L-isoleucyl$>L-histidyl$>L-prolyl$>L-phenylalanin-methylester-hydrochlorid;

DOI:10.1021/ja01578a030

Reference yield:

N-(benzyloxycarbonyl)-L-aspartic acid 4-methyl ester (3160-47-2) → N-benzyloxycarbonyl-O-methyl-L-α-aspartyl=>Nω-nitro-L-arginyl=>L-valyl=>L-tyrosyl=>L-isoleucyl=>L-histidyl=>L-prolyl=>L-phenylalanine-methyl ester (133103-10-3)

Guidance literature:

Multi-step reaction with 2 steps

1: tributylamine; chlorocarbonic acid ethyl ester; THF / Reagens 4: Dioxan; anschliessend Behandeln mit N^ω-Nitro-L-arginin und wss. NaOH

2: aufeinanderfolgendes Behandeln mit Tributylamin und Chlorokohlensaeure-aethylester in Dioxan und mit L-valyl$>L-tyrosyl$>L-isoleucyl$>L-histidyl$>L-prolyl$>L-phenylalanin-methylester-hydrochlorid

With tetrahydrofuran; tributyl-amine; chloroformic acid ethyl ester;

DOI:10.1021/ja01578a030

upstream raw materials:

N-(benzyloxycarbonyl)-L-aspartic acid 4-methyl ester

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