3-Phenyl-1-[tri(propan-2-yl)silyl]-1H-pyrrole

Base Information

Chemical Name:3-Phenyl-1-[tri(propan-2-yl)silyl]-1H-pyrrole
CAS No.:138900-57-9
Molecular Formula:C19H29NSi
Molecular Weight:299.531
Hs Code.:
DSSTox Substance ID:DTXSID20569109
Nikkaji Number:J461.550F
Mol file:138900-57-9.mol

Synonyms:138900-57-9;3-Phenyl-1-[tri(propan-2-yl)silyl]-1H-pyrrole;DTXSID20569109

Suppliers and Price of 3-Phenyl-1-[tri(propan-2-yl)silyl]-1H-pyrrole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3-Phenyl-1-[tri(propan-2-yl)silyl]-1H-pyrrole

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:5
Exact Mass:299.206926464
Heavy Atom Count:21
Complexity:296

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)[Si](C(C)C)(C(C)C)N1C=CC(=C1)C2=CC=CC=C2

Technology Process of 3-Phenyl-1-[tri(propan-2-yl)silyl]-1H-pyrrole

There total 8 articles about 3-Phenyl-1-[tri(propan-2-yl)silyl]-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 591-50-4
iodobenzene

: 138900-55-7
1-(triisopropylsilyl)-1H-pyrrole-3-boronic acid

: 138900-57-9
3-phenyl-1-[tris(propan-2-yl)silyl]-1H-pyrrole

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; benzene; for 16h; Heating;
DOI:10.1021/jo00032a011

Reference yield: 84.0%

: 87630-36-2
3-bromo-1-triisopropylsilanyl-1H-pyrrole

: 591-51-5
phenyllithium

: 138900-57-9
3-phenyl-1-[tris(propan-2-yl)silyl]-1H-pyrrole

Guidance literature:: 3-bromo-1-triisopropylsilanyl-1H-pyrrole; With bis(tri-t-butylphosphine)palladium⁽⁰⁾; oxygen; In toluene; at 20 ℃; for 0.0166667h; Schlenk technique;

phenyllithium; In toluene; at 20 ℃; for 0.0833333h; Schlenk technique;
DOI:10.1002/anie.201700417

Reference yield: 80.0%

: 108-86-1,52753-63-6
bromobenzene

: 168840-90-2
(1-(triisopropylsilyl)-1H-pyrrol-3-yl)magnesium bromide

: 138900-57-9
3-phenyl-1-[tris(propan-2-yl)silyl]-1H-pyrrole

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; 4-methoxyphenyl magnesium bromide; In tetrahydrofuran; at 20 ℃; for 1.5h;
DOI:10.1007/BF00699023