Technology Process of (E,E,E,E)-<2,7-Dimethyl-9-(2,6,6-trimethylcycloxhex-1-enyl)nona-2,4,6,8-tetraenyl>sulfonylbenzene
There total 7 articles about (E,E,E,E)-<2,7-Dimethyl-9-(2,6,6-trimethylcycloxhex-1-enyl)nona-2,4,6,8-tetraenyl>sulfonylbenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: methanol / 17 h / Ambient temperature
2: NaOEt / CH2Cl2; ethanol / 1 h / 0 °C
3: 20percent H2SO4 / acetone / 1 h / 0 °C
4: NaBH4 / methanol / 0.17 h / 0 °C
5: pyridine / 16 h / Ambient temperature
6: propan-2-ol; H2O / Heating
With
pyridine; sodium tetrahydroborate; sulfuric acid; sodium ethanolate;
In
methanol; ethanol; dichloromethane; water; isopropyl alcohol; acetone;
DOI:10.1039/P19930000987
- Guidance literature:
-
Multi-step reaction with 3 steps
1: NaBH4 / methanol / 0.17 h / 0 °C
2: pyridine / 16 h / Ambient temperature
3: propan-2-ol; H2O / Heating
With
pyridine; sodium tetrahydroborate;
In
methanol; water; isopropyl alcohol;
DOI:10.1039/P19930000987
- Guidance literature:
-
Multi-step reaction with 7 steps
1: LiAlH4 / diethyl ether / 0.25 h / Ambient temperature
2: methanol / 17 h / Ambient temperature
3: NaOEt / CH2Cl2; ethanol / 1 h / 0 °C
4: 20percent H2SO4 / acetone / 1 h / 0 °C
5: NaBH4 / methanol / 0.17 h / 0 °C
6: pyridine / 16 h / Ambient temperature
7: propan-2-ol; H2O / Heating
With
pyridine; sodium tetrahydroborate; lithium aluminium tetrahydride; sulfuric acid; sodium ethanolate;
In
methanol; diethyl ether; ethanol; dichloromethane; water; isopropyl alcohol; acetone;
DOI:10.1039/P19930000987
