C₂₃H₂₄N₈O₆S

Base Information

• Chemical Name: C₂₃H₂₄N₈O₆S
• CAS No.: 1367695-15-5
• Molecular Formula: C₂₃H₂₄N₈O₆S
• Molecular Weight: 540.56
• Mol file: 1367695-15-5.mol

Synonyms:

Chemical Property of C₂₃H₂₄N₈O₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₂₄N₈O₆S

There total 4 articles about C₂₃H₂₄N₈O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C27H32N8O6S → C23H24N8O6S (1367695-15-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane;

DOI:10.2174/157018011795514258

Reference yield:

5-((trimethylsilyl)ethynyl)-1H-pyrrolo[2,3-b]pyridine (1207351-09-4) → C23H24N8O6S (1367695-15-5)

Guidance literature:

Multi-step reaction with 3 steps

1: methanol; potassium carbonate / 3 h

2: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol / 0.03 h / Microwave irradiation

3: trifluoroacetic acid / dichloromethane

With methanol; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; trifluoroacetic acid; In dichloromethane; water; tert-butyl alcohol; 2: Huisgen cycloaddition;

DOI:10.2174/157018011795514258

Reference yield:

C15H23N3O5S → C23H24N8O6S (1367695-15-5)

Guidance literature:

Multi-step reaction with 3 steps

1: 1-hydroxy-7-aza-benzotriazole; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide

2: copper(II) sulfate; sodium L-ascorbate / water; tert-butyl alcohol / 0.03 h / Microwave irradiation

3: trifluoroacetic acid / dichloromethane

With 1-hydroxy-7-aza-benzotriazole; copper(II) sulfate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; water; tert-butyl alcohol; 2: Huisgen cycloaddition;

DOI:10.2174/157018011795514258

upstream raw materials:

5-((trimethylsilyl)ethynyl)-1H-pyrrolo[2,3-b]pyridine

tert-butyl 5-ethynyl-1H-pyrrolo[2,3-b]pyridine

C₁₈H₂₆N₆O₆S