2-phenylpent-4-enyl hydroperoxide

Base Information

Chemical Name:2-phenylpent-4-enyl hydroperoxide
CAS No.:126773-70-4
Molecular Formula:C₁₁H₁₄O₂
Molecular Weight:178.231
Hs Code.:

Synonyms:

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Chemical Property of 2-phenylpent-4-enyl hydroperoxide

Chemical Property:

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Technology Process of 2-phenylpent-4-enyl hydroperoxide

There total 5 articles about 2-phenylpent-4-enyl hydroperoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 132637-56-0
N-(2-phenylpent-4-enyl)-N'-p-tosylhydrazine

: 126773-70-4
2-phenylpent-4-enyl hydroperoxide

Guidance literature:: With sodium peroxide; dihydrogen peroxide; In tetrahydrofuran; for 24h; Yield given; Ambient temperature;
DOI:10.1039/P19900002951

Reference yield:

: 96-09-3
styrene oxide

: 126773-70-4
2-phenylpent-4-enyl hydroperoxide

Guidance literature:: Multi-step reaction with 5 steps

1: 52 percent / diethyl ether

2: 65 percent / pyridinium chlorochromate / CH₂Cl₂ / 18 h

3: 42 percent / ethanol / 40 - 50 °C

4: sodium cyanoborohydride, toluene-p-sulphonic acid / tetrahydrofuran / 4 h / pH 3.5

5: 30percent aq. hydrogen peroxide, sodium peroxide / tetrahydrofuran / 24 h / Ambient temperature

With sodium peroxide; dihydrogen peroxide; sodium cyanoborohydride; toluene-4-sulfonic acid; pyridinium chlorochromate; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
DOI:10.1039/P19900002951

Reference yield:

: 24401-36-3
2-phenyl-4-penten-1-al

: 126773-70-4
2-phenylpent-4-enyl hydroperoxide

Guidance literature:: Multi-step reaction with 3 steps

1: 42 percent / ethanol / 40 - 50 °C

2: sodium cyanoborohydride, toluene-p-sulphonic acid / tetrahydrofuran / 4 h / pH 3.5

3: 30percent aq. hydrogen peroxide, sodium peroxide / tetrahydrofuran / 24 h / Ambient temperature

With sodium peroxide; dihydrogen peroxide; sodium cyanoborohydride; toluene-4-sulfonic acid; In tetrahydrofuran; ethanol;
DOI:10.1039/P19900002951