C₃₀H₃₇N₃O₄S

Base Information

Chemical Name:C₃₀H₃₇N₃O₄S
CAS No.:1404377-99-6
Molecular Formula:C₃₀H₃₇N₃O₄S
Molecular Weight:535.707
Hs Code.:

C<sub>30</sub>H<sub>37</sub>N<sub>3</sub>O<sub>4</sub>S

Synonyms:

Suppliers and Price of C₃₀H₃₇N₃O₄S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₀H₃₇N₃O₄S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₀H₃₇N₃O₄S

There total 27 articles about C₃₀H₃₇N₃O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 646-07-1
4-Methylpentanoic acid

: 1404377-99-6
C₃₀H₃₇N₃O₄S

Guidance literature:: Multi-step reaction with 22 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

2.1: 1,1,3,3-Tetramethyldisiloxane / (Ph₃P)2IrCl(CO) / toluene / 2 h / 20 °C

3.1: hydroquinone / acetonitrile / 95 °C

4.1: methyl p-toluene sulfonate / water / 2 h / 110 °C

4.2: 4 h / 95 °C

5.1: hydrogen / rhodium contaminated with carbon / tetrahydrofuran / 7 h / 20 °C / 760.05 Torr

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

7.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C

7.2: Cooling with ice

8.1: triphenylphosphine / dichloromethane / 0.33 h / Cooling with ice

8.2: 0.33 h / Cooling with ice

9.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C

9.2: 1 h / Cooling with ice

10.1: pyridine / methanol / 20 °C

11.1: iodine / acetonitrile / 3 h

12.1: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 80 °C / Inert atmosphere

13.1: trifluoroacetic acid / chloroform

14.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; ammonium chloride / water

15.1: hydrogenchloride; hydrogen / palladium on activated charcoal / water; tetrahydrofuran

16.1: 1H-imidazole / N,N-dimethyl-formamide

17.1: Lawessons reagent / tetrahydrofuran

18.1: ethanol / Molecular sieve

19.1: tetrabutyl ammonium fluoride; acetic acid / water; tetrahydrofuran

20.1: sodium hypochlorite; sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile; water / Phosphate buffer

21.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / water

22.1: sodium hydroxide / ethanol; water; tetrahydrofuran

With Lawessons reagent; pyridine; 1H-imidazole; hydrogenchloride; sodium hypochlorite; sodium chlorite; potassium phosphate; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 1,1,3,3-Tetramethyldisiloxane; tetrabutyl ammonium fluoride; hydrogen; iodine; diisobutylaluminium hydride; ammonium chloride; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinone; methyl p-toluene sulfonate; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; palladium on activated charcoal; rhodium contaminated with carbon; (Ph₃P)2IrCl(CO); In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 1342956-55-1
4-methyl-1-piperidine-1-ylpentan-1-one

: 1404377-99-6
C₃₀H₃₇N₃O₄S

Guidance literature:: Multi-step reaction with 21 steps

1.1: 1,1,3,3-Tetramethyldisiloxane / (Ph₃P)2IrCl(CO) / toluene / 2 h / 20 °C

2.1: hydroquinone / acetonitrile / 95 °C

3.1: methyl p-toluene sulfonate / water / 2 h / 110 °C

3.2: 4 h / 95 °C

4.1: hydrogen / rhodium contaminated with carbon / tetrahydrofuran / 7 h / 20 °C / 760.05 Torr

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

6.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C

6.2: Cooling with ice

7.1: triphenylphosphine / dichloromethane / 0.33 h / Cooling with ice

7.2: 0.33 h / Cooling with ice

8.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C

8.2: 1 h / Cooling with ice

9.1: pyridine / methanol / 20 °C

10.1: iodine / acetonitrile / 3 h

11.1: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 80 °C / Inert atmosphere

12.1: trifluoroacetic acid / chloroform

13.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; ammonium chloride / water

14.1: hydrogenchloride; hydrogen / palladium on activated charcoal / water; tetrahydrofuran

15.1: 1H-imidazole / N,N-dimethyl-formamide

16.1: Lawessons reagent / tetrahydrofuran

17.1: ethanol / Molecular sieve

18.1: tetrabutyl ammonium fluoride; acetic acid / water; tetrahydrofuran

19.1: sodium hypochlorite; sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile; water / Phosphate buffer

20.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / water

21.1: sodium hydroxide / ethanol; water; tetrahydrofuran

With Lawessons reagent; pyridine; 1H-imidazole; hydrogenchloride; sodium hypochlorite; sodium chlorite; potassium phosphate; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 1,1,3,3-Tetramethyldisiloxane; tetrabutyl ammonium fluoride; hydrogen; iodine; diisobutylaluminium hydride; ammonium chloride; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinone; methyl p-toluene sulfonate; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; palladium on activated charcoal; rhodium contaminated with carbon; (Ph₃P)2IrCl(CO); In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; chloroform; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 1404378-77-3
ethyl 3-isobutyl-2-piperidine-1-ylcyclobutanecarboxylate

: 1404377-99-6
C₃₀H₃₇N₃O₄S

Guidance literature:: Multi-step reaction with 19 steps

1.1: methyl p-toluene sulfonate / water / 2 h / 110 °C

1.2: 4 h / 95 °C

2.1: hydrogen / rhodium contaminated with carbon / tetrahydrofuran / 7 h / 20 °C / 760.05 Torr

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

4.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C

4.2: Cooling with ice

5.1: triphenylphosphine / dichloromethane / 0.33 h / Cooling with ice

5.2: 0.33 h / Cooling with ice

6.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C

6.2: 1 h / Cooling with ice

7.1: pyridine / methanol / 20 °C

8.1: iodine / acetonitrile / 3 h

9.1: potassium phosphate / bis-triphenylphosphine-palladium(II) chloride / N,N-dimethyl-formamide; water / 80 °C / Inert atmosphere

10.1: trifluoroacetic acid / chloroform

11.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; ammonium chloride / water

12.1: hydrogenchloride; hydrogen / palladium on activated charcoal / water; tetrahydrofuran

13.1: 1H-imidazole / N,N-dimethyl-formamide

14.1: Lawessons reagent / tetrahydrofuran

15.1: ethanol / Molecular sieve

16.1: tetrabutyl ammonium fluoride; acetic acid / water; tetrahydrofuran

17.1: sodium hypochlorite; sodium chlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile; water / Phosphate buffer

18.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / water

19.1: sodium hydroxide / ethanol; water; tetrahydrofuran

With Lawessons reagent; pyridine; 1H-imidazole; hydrogenchloride; sodium hypochlorite; sodium chlorite; potassium phosphate; n-butyllithium; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl ammonium fluoride; hydrogen; iodine; diisobutylaluminium hydride; ammonium chloride; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; methyl p-toluene sulfonate; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; bis-triphenylphosphine-palladium(II) chloride; palladium on activated charcoal; rhodium contaminated with carbon; In tetrahydrofuran; methanol; ethanol; hexane; dichloromethane; chloroform; water; N,N-dimethyl-formamide; acetonitrile;