[((C₆H₅)2PCH₂)2(Cl)Fe((CH₃CH₂)2C₂B₄H₄)]

Base Information

Chemical Name:[((C₆H₅)2PCH₂)2(Cl)Fe((CH₃CH₂)2C₂B₄H₄)]
CAS No.:98330-40-6
Molecular Formula:C₃₂H₃₈B₄ClFeP₂
Molecular Weight:619.145
Hs Code.:

[((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>)2(Cl)Fe((CH<sub>3</sub>CH<sub>2</sub>)2C<sub>2</sub>B<sub>4</sub>H<sub>4</sub>)]

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [((C₆H₅)2PCH₂)2(Cl)Fe((CH₃CH₂)2C₂B₄H₄)]

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Technology Process of [((C₆H₅)2PCH₂)2(Cl)Fe((CH₃CH₂)2C₂B₄H₄)]

There total 1 articles about [((C₆H₅)2PCH₂)2(Cl)Fe((CH₃CH₂)2C₂B₄H₄)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 80583-48-8
1,2-diethyl-nido-carborane

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: iron(II) chloride

: 98330-40-6
[((C₆H₅)2PCH₂)2(Cl)Fe((CH₃CH₂)2C₂B₄H₄)]

Guidance literature:: With NaH; In tetrahydrofuran; preparation of Na(C2H5)2C2B4H5 from NaH/THF and (C2H5)2C2B4H6; filtration into an at -196°C cooled flask with FeCl2, phosphine; addn. ofTHF; warming at room temp.; stirring, 4-15h, producing an orange-red soln.;; removal of solvent; dissolving of residue in a minimum volume of CH2Cl2; chromy. on silica gel column packed in hexane; elution with 50% acetone/hexane, resulting a red-orange soln.; rotary evapn.; thin-layer chromy. of red solid in 50% CH2Cl2/hexane;;