C₃₆H₄₂ClN₃O₃S

Base Information

Chemical Name:C₃₆H₄₂ClN₃O₃S
CAS No.:1382034-68-5
Molecular Formula:C₃₆H₄₂ClN₃O₃S
Molecular Weight:632.267
Hs Code.:

C<sub>36</sub>H<sub>42</sub>ClN<sub>3</sub>O<sub>3</sub>S

Synonyms:

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Chemical Property of C₃₆H₄₂ClN₃O₃S

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Technology Process of C₃₆H₄₂ClN₃O₃S

There total 9 articles about C₃₆H₄₂ClN₃O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1382034-59-4
(3-bromoadamantan-1-yl)methanesulfonamide

: 1382034-68-5
C₃₆H₄₂ClN₃O₃S

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium dihydrogenphosphate / water / 0.17 h / 180 °C / Microwave irradiation; Inert atmosphere

2.1: diethylamino-sulfur trifluoride / dichloromethane / 24 h / 20 °C / Inert atmosphere

3.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With sodium dihydrogenphosphate; diethylamino-sulfur trifluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ml300095a

Reference yield:

: 1382034-60-7
(3-hydroxyadamantan-1-yl)methanesulfonamide

: 1382034-68-5
C₃₆H₄₂ClN₃O₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: diethylamino-sulfur trifluoride / dichloromethane / 24 h / 20 °C / Inert atmosphere

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With diethylamino-sulfur trifluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ml300095a

Reference yield:

: C₁₃H₁₉BrOS

: 1382034-68-5
C₃₆H₄₂ClN₃O₃S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sulfuryl dichloride; acetic anhydride / 1,2-dichloro-ethane / 0.5 h / -10 °C / Inert atmosphere

1.2: Inert atmosphere; Cooling with ice

2.1: potassium permanganate / water; acetone / 2 h / 50 °C / Inert atmosphere

3.1: sodium dihydrogenphosphate / water / 0.17 h / 180 °C / Microwave irradiation; Inert atmosphere

4.1: diethylamino-sulfur trifluoride / dichloromethane / 24 h / 20 °C / Inert atmosphere

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

5.2: 20 °C / Inert atmosphere

6.1: dichloromethane / 0.5 h / 20 °C / Inert atmosphere

With potassium permanganate; sodium dihydrogenphosphate; sulfuryl dichloride; diethylamino-sulfur trifluoride; acetic anhydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ml300095a