ReO(N,N'-di-o-tolylthiourea)2Cl3

Base Information

• Chemical Name: ReO(N,N'-di-o-tolylthiourea)2Cl3
• CAS No.: 330548-33-9
• Molecular Formula: C₃₀H₃₂Cl₃N₄OReS₂
• Molecular Weight: 821.308

Synonyms:

Chemical Property of ReO(N,N'-di-o-tolylthiourea)2Cl3

Chemical Property:

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Technology Process of ReO(N,N'-di-o-tolylthiourea)2Cl3

There total 1 articles about ReO(N,N'-di-o-tolylthiourea)2Cl3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

oxopentachlororhenic acid + N,N'-di(o-tolyl)thiourea (137-97-3) → ReO(N,N'-di-o-tolylthiourea)2Cl3 (330548-33-9)

Guidance literature:

In hydrogenchloride; adding soln. of the ligand in acetone or ethanol with molar ratio Re : L= 1 : 2 to 0.1 M soln. of H2(ReOCl5) in concd. HCl; filtering pptd. crystals off, washing with HCl and n-propanol, drying over CaCl2; elem. anal.;

DOI:10.1007/BF02496343

upstream raw materials:

N,N'-di(o-tolyl)thiourea

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