tert-Butyl-[(3aR,4R,7aR)-4-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-3a,7a-dihydro-4H-[1,3]dioxolo[4,5-c]pyran-6-ylmethoxy]-diphenyl-silane

Base Information

Chemical Name:tert-Butyl-[(3aR,4R,7aR)-4-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-3a,7a-dihydro-4H-[1,3]dioxolo[4,5-c]pyran-6-ylmethoxy]-diphenyl-silane
CAS No.:132820-95-2
Molecular Formula:C₃₀H₄₀O₆Si
Molecular Weight:524.73
Hs Code.:

tert-Butyl-[(3aR,4R,7aR)-4-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-3a,7a-dihydro-4H-[1,3]dioxolo[4,5-c]pyran-6-ylmethoxy]-diphenyl-silane

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Chemical Property of tert-Butyl-[(3aR,4R,7aR)-4-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-3a,7a-dihydro-4H-[1,3]dioxolo[4,5-c]pyran-6-ylmethoxy]-diphenyl-silane

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Technology Process of tert-Butyl-[(3aR,4R,7aR)-4-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-3a,7a-dihydro-4H-[1,3]dioxolo[4,5-c]pyran-6-ylmethoxy]-diphenyl-silane

There total 4 articles about tert-Butyl-[(3aR,4R,7aR)-4-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-3a,7a-dihydro-4H-[1,3]dioxolo[4,5-c]pyran-6-ylmethoxy]-diphenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 60920-73-2
benzyl 2-acetamido-3-O-allyl-2-deoxy-α-D-glucopyranoside

: 132820-90-7
(3aR,4R,6R,7aR)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-4-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-ol

: 132820-95-2
tert-Butyl-[(3aR,4R,7aR)-4-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-3a,7a-dihydro-4H-[1,3]dioxolo[4,5-c]pyran-6-ylmethoxy]-diphenyl-silane

: 132820-94-1
C₄₈H₆₅NO₁₂Si

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; for 5.5h; Heating;

Reference yield: 70.0%

: 132820-90-7
(3aR,4R,6R,7aR)-6-(tert-Butyl-diphenyl-silanyloxymethyl)-4-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-ol

: 4064-06-6
1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: 132820-95-2
tert-Butyl-[(3aR,4R,7aR)-4-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-3a,7a-dihydro-4H-[1,3]dioxolo[4,5-c]pyran-6-ylmethoxy]-diphenyl-silane

: 132820-92-9
C₄₂H₆₀O₁₂Si

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; for 2.5h; Heating;

Reference yield:

: 125884-17-5
4,5:7,8-di-O-isopropylidene-3-deoxy-D-manno-2-octulose

: 132820-95-2
tert-Butyl-[(3aR,4R,7aR)-4-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-2,2-dimethyl-3a,7a-dihydro-4H-[1,3]dioxolo[4,5-c]pyran-6-ylmethoxy]-diphenyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / imidazole

2: 13 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 5.5 h / Heating

With 1H-imidazole; pyridinium p-toluenesulfonate; In dichloromethane;