C₃₄H₄₆O₄Si

Base Information

Chemical Name:C₃₄H₄₆O₄Si
CAS No.:1432425-62-1
Molecular Formula:C₃₄H₄₆O₄Si
Molecular Weight:546.822
Hs Code.:

C<sub>34</sub>H<sub>46</sub>O<sub>4</sub>Si

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₄H₄₆O₄Si

Chemical Property:

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Technology Process of C₃₄H₄₆O₄Si

There total 17 articles about C₃₄H₄₆O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1432425-59-6
C₃₄H₄₆O₄Si

: 1432425-62-1
C₃₄H₄₆O₄Si

Guidance literature:: With silica gel; In hexane; ethyl acetate;
DOI:10.1016/j.bmcl.2013.03.024

Reference yield:

: C₃₈H₅₆O₅Si

: 1432425-62-1
C₃₄H₄₆O₄Si

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / tetrahydrofuran; water

2: Dess-Martin periodane / dichloromethane

3: silica gel / ethyl acetate; hexane

With silica gel; Dess-Martin periodane; acetic acid; In tetrahydrofuran; hexane; dichloromethane; water; ethyl acetate; 2: |Dess-Martin Oxidation;
DOI:10.1016/j.bmcl.2013.03.024

Reference yield:

: C₂₈H₃₈O₅Si

: 1432425-62-1
C₃₄H₄₆O₄Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C

2.1: potassium carbonate / methanol / 19 h / 20 - 45 °C

3.1: triethylamine; dmap / dichloromethane / 1.5 h / 20 °C

4.1: copper(l) iodide / acetonitrile / 24 h / 20 °C

5.1: platinum(IV) oxide; hydrogen / ethyl acetate / 3 h / 20 °C

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 22.5 h / 0 - 20 °C

7.1: oxalyl dichloride; dimethyl sulfoxide / 0.25 h / -78 °C

7.2: 0.75 h / 0 °C

8.1: sodium hydride / tetrahydrofuran / 0 - 20 °C

9.1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.17 h / -20 °C

10.1: 1H-imidazole; triethylamine; dmap / N,N-dimethyl-formamide

11.1: sodium hydroxide / methanol; water

12.1: triphenylphosphine / benzene / Reflux

13.1: acetic acid / tetrahydrofuran; water

14.1: Dess-Martin periodane / dichloromethane

15.1: silica gel / ethyl acetate; hexane

With 1H-imidazole; dmap; platinum(IV) oxide; sodium tetrahydroborate; copper(l) iodide; oxalyl dichloride; cerium(III) chloride heptahydrate; tetrabutyl ammonium fluoride; hydrogen; silica gel; sodium hydride; diisobutylaluminium hydride; potassium carbonate; Dess-Martin periodane; acetic acid; dimethyl sulfoxide; triethylamine; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; hexane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; benzene; 7.2: |Swern Oxidation / 8.1: |Horner-Wadsworth-Emmons Olefination / 14.1: |Dess-Martin Oxidation;
DOI:10.1016/j.bmcl.2013.03.024