1-(4-Methoxy-benzyl)-5-{3-(4-methoxy-benzyl)-5-[(Z)-4-methoxy-phenylimino]-3,5-dihydro-[1,2,3]triazolo[4,5-d]pyrimidin-6-yl}-1H-[1,2,3]triazole-4-carbaldehyde

Base Information

Chemical Name:1-(4-Methoxy-benzyl)-5-{3-(4-methoxy-benzyl)-5-[(Z)-4-methoxy-phenylimino]-3,5-dihydro-[1,2,3]triazolo[4,5-d]pyrimidin-6-yl}-1H-[1,2,3]triazole-4-carbaldehyde
CAS No.:115462-15-2
Molecular Formula:C₃₀H₂₇N₉O₄
Molecular Weight:577.602
Hs Code.:

1-(4-Methoxy-benzyl)-5-{3-(4-methoxy-benzyl)-5-[(Z)-4-methoxy-phenylimino]-3,5-dihydro-[1,2,3]triazolo[4,5-d]pyrimidin-6-yl}-1H-[1,2,3]triazole-4-carbaldehyde

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Chemical Property of 1-(4-Methoxy-benzyl)-5-{3-(4-methoxy-benzyl)-5-[(Z)-4-methoxy-phenylimino]-3,5-dihydro-[1,2,3]triazolo[4,5-d]pyrimidin-6-yl}-1H-[1,2,3]triazole-4-carbaldehyde

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Technology Process of 1-(4-Methoxy-benzyl)-5-{3-(4-methoxy-benzyl)-5-[(Z)-4-methoxy-phenylimino]-3,5-dihydro-[1,2,3]triazolo[4,5-d]pyrimidin-6-yl}-1H-[1,2,3]triazole-4-carbaldehyde

There total 3 articles about 1-(4-Methoxy-benzyl)-5-{3-(4-methoxy-benzyl)-5-[(Z)-4-methoxy-phenylimino]-3,5-dihydro-[1,2,3]triazolo[4,5-d]pyrimidin-6-yl}-1H-[1,2,3]triazole-4-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 5416-93-3
4-Methoxyphenyl isocyanate

: 115437-57-5
4-formyl-1-(p-methoxybenzyl)-5-<(triphenylphosphoranylidene)amino>-1H-<1,2,3>triazole

: 115462-15-2
1-(4-Methoxy-benzyl)-5-{3-(4-methoxy-benzyl)-5-[(Z)-4-methoxy-phenylimino]-3,5-dihydro-[1,2,3]triazolo[4,5-d]pyrimidin-6-yl}-1H-[1,2,3]triazole-4-carbaldehyde

Guidance literature:: In toluene; for 5h; Heating;
DOI:10.1021/jo00255a003

Reference yield:

: 97326-47-1
5-chloro-4-formyl-1-(p-methoxybenzyl)-1H-<1,2,3>triazole

: 115462-15-2
1-(4-Methoxy-benzyl)-5-{3-(4-methoxy-benzyl)-5-[(Z)-4-methoxy-phenylimino]-3,5-dihydro-[1,2,3]triazolo[4,5-d]pyrimidin-6-yl}-1H-[1,2,3]triazole-4-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / sodium azide / dimethylsulfoxide / 1 h / 60 °C

2: 90 percent / CH₂Cl₂ / 16 h / Ambient temperature

3: 31 percent / toluene / 5 h / Heating

With sodium azide; In dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/jo00255a003

Reference yield:

: 115437-25-7
5-azido-4-formyl-1-(p-methoxybenzyl)-1H-<1,2,3>triazole

: 115462-15-2
1-(4-Methoxy-benzyl)-5-{3-(4-methoxy-benzyl)-5-[(Z)-4-methoxy-phenylimino]-3,5-dihydro-[1,2,3]triazolo[4,5-d]pyrimidin-6-yl}-1H-[1,2,3]triazole-4-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / CH₂Cl₂ / 16 h / Ambient temperature

2: 31 percent / toluene / 5 h / Heating

In dichloromethane; toluene;
DOI:10.1021/jo00255a003