Methyl 2,4-di-O-benzyl-3-O-<2,3,6-tri-O-benzyl-4-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranoside 3''-(1,2-di-O-benzyl-sn-glycer-3-yl-triethylammonium phosphate)

Base Information

• Chemical Name: Methyl 2,4-di-O-benzyl-3-O-<2,3,6-tri-O-benzyl-4-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranoside 3''-(1,2-di-O-benzyl-sn-glycer-3-yl-triethylammonium phosphate)
• CAS No.: 141263-16-3
• Molecular Formula: C₆H₁₅N*C₇₇H₈₉O₂₃P
• Molecular Weight: 1514.71

Synonyms:

Chemical Property of Methyl 2,4-di-O-benzyl-3-O-<2,3,6-tri-O-benzyl-4-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranoside 3''-(1,2-di-O-benzyl-sn-glycer-3-yl-triethylammonium phosphate)

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Technology Process of Methyl 2,4-di-O-benzyl-3-O-<2,3,6-tri-O-benzyl-4-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranoside 3''-(1,2-di-O-benzyl-sn-glycer-3-yl-triethylammonium phosphate)

There total 1 articles about Methyl 2,4-di-O-benzyl-3-O-<2,3,6-tri-O-benzyl-4-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranoside 3''-(1,2-di-O-benzyl-sn-glycer-3-yl-triethylammonium phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triethylamine carbonate (15715-58-9) + Methyl 2,4-di-O-benzyl-3-O-<2,3,6-tri-O-benzyl-4-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranoside 3''-(1,2-di-O-benzyl-sn-glycer-3-yl phosphonate) (141263-14-1) → Methyl 2,4-di-O-benzyl-3-O-<2,3,6-tri-O-benzyl-4-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranoside 3''-(1,2-di-O-benzyl-sn-glycer-3-yl-triethylammonium phosphate) (141263-16-3)

Guidance literature:

With iodine; Yield given. Multistep reaction; 1) THF - pyridine - water, 3 h;

DOI:10.1016/S0008-6215(00)90498-1

Reference yield:

Methyl 2,4-di-O-benzyl-3-O-<2,3,6-tri-O-benzyl-4-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranoside 3''-(1,2-di-O-benzyl-sn-glycer-3-yl-triethylammonium phosphate) (141263-16-3) → C71H83O20P*C6H15N

Guidance literature:

With ammonium hydroxide; In methanol; dichloromethane; for 72h;

DOI:10.1016/S0008-6215(00)90498-1

upstream raw materials:

triethylamine carbonate

Methyl 2,4-di-O-benzyl-3-O-<2,3,6-tri-O-benzyl-4-O-(2,4,6-tri-O-acetyl-β-D-galactopyranosyl)-α-D-glucopyranosyl>-α-L-rhamnopyranoside 3''-(1,2-di-O-benzyl-sn-glycer-3-yl phosphonate)

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