C₁₅H₂₀F₂N₂O

Base Information

Chemical Name:C₁₅H₂₀F₂N₂O
CAS No.:1292322-05-4
Molecular Formula:C₁₅H₂₀F₂N₂O
Molecular Weight:282.333
Hs Code.:

C<sub>15</sub>H<sub>20</sub>F<sub>2</sub>N<sub>2</sub>O

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₀F₂N₂O

Chemical Property:

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Technology Process of C₁₅H₂₀F₂N₂O

There total 12 articles about C₁₅H₂₀F₂N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₂₈F₂N₂O₃

: 1292322-05-4
C₁₅H₂₀F₂N₂O

Guidance literature:: With hydrogenchloride; In methanol; at 20 ℃;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: C₁₄H₂₀Cl₃NO₅

: 1292322-05-4
C₁₅H₂₀F₂N₂O

Guidance literature:: Multi-step reaction with 10 steps

1: n-butyllithium / tetrahydrofuran / -78 °C

2: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C

3: hydrogenchloride / methanol / 20 °C

4: triethylamine / dichloromethane / 20 °C

5: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C

6: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 100 °C

7: chloro-trimethyl-silane / dichloromethane / 20 °C

8: palladium 10% on activated carbon; hydrogen / ethanol

9: triethylamine / dichloromethane / 20 °C

10: hydrogenchloride / methanol / 20 °C

With hydrogenchloride; n-butyllithium; chloro-trimethyl-silane; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; sodium hexamethyldisilazane; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 6: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060

Reference yield:

: 1292321-47-1
C₂₉H₃₄F₂N₂O₅

: 1292322-05-4
C₁₅H₂₀F₂N₂O

Guidance literature:: Multi-step reaction with 8 steps

1: hydrogenchloride / methanol / 20 °C

2: triethylamine / dichloromethane / 20 °C

3: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 20 °C

4: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / toluene / 100 °C

5: chloro-trimethyl-silane / dichloromethane / 20 °C

6: palladium 10% on activated carbon; hydrogen / ethanol

7: triethylamine / dichloromethane / 20 °C

8: hydrogenchloride / methanol / 20 °C

With hydrogenchloride; chloro-trimethyl-silane; diphenyl phosphoryl azide; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; 4: Curtius rearrangement;
DOI:10.1016/j.bmcl.2010.12.060