dizinc μ-benzohydroxamate (μ-CH3CO2)2(CH3CO2)(((CH3)2NCH2)2)

Base Information

Chemical Name:dizinc μ-benzohydroxamate (μ-CH3CO2)2(CH3CO2)(((CH3)2NCH2)2)
CAS No.:448212-51-9
Molecular Formula:C₁₉H₃₁N₃O₈Zn₂
Molecular Weight:560.25
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dizinc μ-benzohydroxamate (μ-CH3CO2)2(CH3CO2)(((CH3)2NCH2)2)

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Technology Process of dizinc μ-benzohydroxamate (μ-CH3CO2)2(CH3CO2)(((CH3)2NCH2)2)

There total 3 articles about dizinc μ-benzohydroxamate (μ-CH3CO2)2(CH3CO2)(((CH3)2NCH2)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.3%

: 858943-58-5,448212-48-4
[Zn(OAc)2(N,N,N',N'-tetramethylethylenediamine)]

: 495-18-1
Benzohydroxamic acid

: bis(benzohydroxamato)zinc(II) hydrate

: 448212-51-9
dizinc μ-benzohydroxamate (μ-CH3CO2)2(CH3CO2)(((CH3)2NCH2)2)

Guidance literature:: In methanol; soln. benzohydroxamic acid in MeOH was added dropwise to soln. zinc complex in MeOH and stirred for 1 h; soln. was filtered and concd. in vacuo, residue was stirred in ether, filtered, and ether washings were left to stand in air; elem. anal.;
DOI:10.1021/ic050849m

Reference yield:

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 448212-51-9
dizinc μ-benzohydroxamate (μ-CH3CO2)2(CH3CO2)(((CH3)2NCH2)2)

Guidance literature:: Multi-step reaction with 2 steps

1: methanol

2: methanol

In methanol;
DOI:10.1021/ic050849m

Reference yield:

: 110-18-9
N,N,N,N,-tetramethylethylenediamine

: 194043-89-5,15633-79-1,81736-05-2
zinc(II) acetate dihydrate

: 495-18-1
Benzohydroxamic acid

: bis(benzohydroxamato)zinc(II) hydrate

: 448212-51-9
dizinc μ-benzohydroxamate (μ-CH3CO2)2(CH3CO2)(((CH3)2NCH2)2)

Guidance literature:: In methanol; diethyl ether; to soln. of Zn acetate and diamine soln. of acid added dropwise, stirredfor 3 h; crystals of Zn((C6H5)C(O)NHO)2 filtered off, soln. stirred in diethyl ether for 1 h; elem. anal.;
DOI:10.1039/b202612k