4,4'-Azoxybistritanol

Base Information

Chemical Name:4,4'-Azoxybistritanol
CAS No.:128527-13-9
Molecular Formula:C₃₈H₃₀N₂O₃
Molecular Weight:562.668
Hs Code.:

Synonyms:

Suppliers and Price of 4,4'-Azoxybistritanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-Azoxybistritanol

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4,4'-Azoxybistritanol

There total 10 articles about 4,4'-Azoxybistritanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 128527-12-8
4,4'-Azobistritanol

: 128527-13-9
4,4'-Azoxybistritanol

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 3h; Heating;

Reference yield:

: 2945-12-2
1-(diphenylmethyl)-4-nitrobenzene

: 128527-13-9
4,4'-Azoxybistritanol

Guidance literature:: Multi-step reaction with 4 steps

1: NaOH, Zn-dust / 2-methoxy-ethanol; methanol; H₂O / 1 h / Heating

2: CrO₃, glacial AcOH / 1) 1 h, 100 deg C 2) 24 h, r.t.

3: 73 percent / conc. HNO₃, NaNO₂ / dioxane; H₂O / 100 °C

4: 73 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 3 h / Heating

With chromium(VI) oxide; sodium hydroxide; nitric acid; acetic acid; 3-chloro-benzenecarboperoxoic acid; zinc; sodium nitrite; In 1,4-dioxane; methanol; dichloromethane; 2-methoxy-ethanol; water;

Reference yield:

: 555-16-8
4-nitrobenzaldehdye

: 128527-13-9
4,4'-Azoxybistritanol

Guidance literature:: Multi-step reaction with 5 steps

1: 69 percent / conc. H₂SO₄ / 48 h

2: NaOH, Zn-dust / 2-methoxy-ethanol; methanol; H₂O / 1 h / Heating

3: CrO₃, glacial AcOH / 1) 1 h, 100 deg C 2) 24 h, r.t.

4: 73 percent / conc. HNO₃, NaNO₂ / dioxane; H₂O / 100 °C

5: 73 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 3 h / Heating

With chromium(VI) oxide; sodium hydroxide; sulfuric acid; nitric acid; acetic acid; 3-chloro-benzenecarboperoxoic acid; zinc; sodium nitrite; In 1,4-dioxane; methanol; dichloromethane; 2-methoxy-ethanol; water;