Technology Process of C49H74N10O10
There total 9 articles about C49H74N10O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
cesium fluoride;
In
acetonitrile;
at 25 ℃;
for 3h;
DOI:10.1039/c1ob05606a
- Guidance literature:
-
Multi-step reaction with 8 steps
1: hydrogenchloride; methanol / 4 h / 50 °C
2: sodium hydroxide / water; dimethyl sulfoxide / 18 h / 25 °C
3: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 25 °C
4: triethylamine / dichloromethane / 4 h / 25 °C
5: sodium azide / N,N-dimethyl-formamide / 72 h / 110 °C
6: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 70 °C
7: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 8 h / 25 °C
8: cesium fluoride / acetonitrile / 3 h / 25 °C
With
hydrogenchloride; methanol; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium azide; triethylamine; N-ethyl-N,N-diisopropylamine; cesium fluoride; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;
3: Huisgen-Sharpless 1,3-dipolar cycloaddition / 6: Huisgen-Sharpless 1,3-dipolar cycloaddition / 7: Sonogashira coupling;
DOI:10.1039/c1ob05606a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper(l) iodide; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 15 h / 70 °C
2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 8 h / 25 °C
3: cesium fluoride / acetonitrile / 3 h / 25 °C
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; N-ethyl-N,N-diisopropylamine; cesium fluoride;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;
1: Huisgen-Sharpless 1,3-dipolar cycloaddition / 2: Sonogashira coupling;
DOI:10.1039/c1ob05606a