methyl-3 (methyl-4 cyclohexene-3 yl)-5 hexene-5 thioate de S-methyle

Base Information

Chemical Name:methyl-3 (methyl-4 cyclohexene-3 yl)-5 hexene-5 thioate de S-methyle
CAS No.:121726-41-8
Molecular Formula:C₁₅H₂₄OS
Molecular Weight:252.421
Hs Code.:

Synonyms:

Suppliers and Price of methyl-3 (methyl-4 cyclohexene-3 yl)-5 hexene-5 thioate de S-methyle

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl-3 (methyl-4 cyclohexene-3 yl)-5 hexene-5 thioate de S-methyle

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl-3 (methyl-4 cyclohexene-3 yl)-5 hexene-5 thioate de S-methyle

There total 4 articles about methyl-3 (methyl-4 cyclohexene-3 yl)-5 hexene-5 thioate de S-methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 121726-39-4,121726-40-7
methyl-3 (methyl-4 cyclohexene-3 yl)-5 N-phenyl hexene-5 imidothioate de methyle

: 121726-41-8,121726-42-9
methyl-3 (methyl-4 cyclohexene-3 yl)-5 hexene-5 thioate de S-methyle

Guidance literature:: With hydrogenchloride; In water; acetonitrile; at 50 ℃; for 4h;

Reference yield:

: 121726-26-9
N-phenyl butene-3 imidothioate de methyle

: 121726-41-8,121726-42-9
methyl-3 (methyl-4 cyclohexene-3 yl)-5 hexene-5 thioate de S-methyle

Guidance literature:: Multi-step reaction with 3 steps

1: 5 percent DBU / tetrahydrofuran / 16 h / Heating

2: 1.) BuLi, TMEDA / 2.) THF, -78 deg C, 2 h

3: 81 percent / 10 percent hydrochloric acid / acetonitrile; H₂O / 4 h / 50 °C

With hydrogenchloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; water; acetonitrile;

Reference yield:

: 65672-29-9,95502-91-3,121726-25-8
N-phenyl butene-2 imidothioate de methyle

: 121726-41-8,121726-42-9
methyl-3 (methyl-4 cyclohexene-3 yl)-5 hexene-5 thioate de S-methyle

Guidance literature:: Multi-step reaction with 3 steps

1: 85 °C / 0.4 Torr

2: 1.) BuLi, TMEDA / 2.) THF, -78 deg C, 2 h

3: 81 percent / 10 percent hydrochloric acid / acetonitrile; H₂O / 4 h / 50 °C

With hydrogenchloride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In water; acetonitrile;