Technology Process of C19H24N6O2
There total 6 articles about C19H24N6O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C
2: potassium carbonate / dimethyl sulfoxide / 80 °C
3: methanol; potassium hydroxide / 1,4-dioxane
With
methanol; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide;
In
1,4-dioxane; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2012.01.019
- Guidance literature:
-
Multi-step reaction with 4 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / -70 - 20 °C
2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C
3: potassium carbonate / dimethyl sulfoxide / 80 °C
4: methanol; potassium hydroxide / 1,4-dioxane
With
methanol; di-isopropyl azodicarboxylate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; potassium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/j.bmcl.2012.01.019