Technology Process of C22H34N4O5S
There total 3 articles about C22H34N4O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 70 percent / thionation reagent (prepared from diphenyl ether and phosphorus pentasulfide) / tetrahydrofuran / 1 h / 0 °C
2: 60 percent / triethylamine, mercuric acetate, hydroxylamine hydrochloride / acetonitrile
With
thionation reagent (prepared from diphenyl ether and phosphorus pentasulfide); hydroxylamine hydrochloride; mercury(II) diacetate; triethylamine;
In
tetrahydrofuran; acetonitrile;
DOI:10.1139/v85-511
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 98percent formic acid / 3 h / Ambient temperature
2: EEDQ / CHCl3 / 8 h / Ambient temperature
3: 70 percent / thionation reagent (prepared from diphenyl ether and phosphorus pentasulfide) / tetrahydrofuran / 1 h / 0 °C
4: 60 percent / triethylamine, mercuric acetate, hydroxylamine hydrochloride / acetonitrile
With
formic acid; thionation reagent (prepared from diphenyl ether and phosphorus pentasulfide); hydroxylamine hydrochloride; mercury(II) diacetate; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine;
In
tetrahydrofuran; chloroform; acetonitrile;
DOI:10.1139/v85-511
- Guidance literature:
-
Multi-step reaction with 3 steps
1: EEDQ / CHCl3 / 8 h / Ambient temperature
2: 70 percent / thionation reagent (prepared from diphenyl ether and phosphorus pentasulfide) / tetrahydrofuran / 1 h / 0 °C
3: 60 percent / triethylamine, mercuric acetate, hydroxylamine hydrochloride / acetonitrile
With
thionation reagent (prepared from diphenyl ether and phosphorus pentasulfide); hydroxylamine hydrochloride; mercury(II) diacetate; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; triethylamine;
In
tetrahydrofuran; chloroform; acetonitrile;
DOI:10.1139/v85-511