Technology Process of C24H29N5O2S
There total 4 articles about C24H29N5O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trifluoroacetic acid / dichloromethane
2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane; water
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid;
In
dichloromethane; water;
DOI:10.1016/j.bmcl.2012.05.130
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium acetate / ethanol / Reflux
2: trifluoroacetic acid / dichloromethane
3: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane; water
With
sodium acetate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid;
In
ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2012.05.130
- Guidance literature:
-
Multi-step reaction with 4 steps
1: water; sodium hydroxide / tetrahydrofuran / 2 h / Reflux
2: sodium acetate / ethanol / Reflux
3: trifluoroacetic acid / dichloromethane
4: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane; water
With
water; sodium acetate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2012.05.130