2-hydroxymethyl-2-(2'-hydroxy-4'-hydroxymethylphenyl)oxirane triisobutyrate

Base Information

Chemical Name:2-hydroxymethyl-2-(2'-hydroxy-4'-hydroxymethylphenyl)oxirane triisobutyrate
CAS No.:64190-69-8
Molecular Formula:C₂₂H₃₀O₇
Molecular Weight:406.476
Hs Code.:

Synonyms:

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Chemical Property of 2-hydroxymethyl-2-(2'-hydroxy-4'-hydroxymethylphenyl)oxirane triisobutyrate

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Technology Process of 2-hydroxymethyl-2-(2'-hydroxy-4'-hydroxymethylphenyl)oxirane triisobutyrate

There total 8 articles about 2-hydroxymethyl-2-(2'-hydroxy-4'-hydroxymethylphenyl)oxirane triisobutyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78069-56-4
Isobutyric acid 5-isobutyryloxymethyl-2-(1-isobutyryloxymethyl-vinyl)-phenyl ester

: 64190-69-8
2-hydroxymethyl-2-(2'-hydroxy-4'-hydroxymethylphenyl)oxirane triisobutyrate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 56h; Ambient temperature;

Reference yield:

: 53878-05-0
7-bromomethyl-4-methylcoumarin

: 64190-69-8
2-hydroxymethyl-2-(2'-hydroxy-4'-hydroxymethylphenyl)oxirane triisobutyrate

Guidance literature:: Multi-step reaction with 6 steps

1: 85 g / acetic acid / 6 h / Heating

2: 1)aq. sodium hydroxide, 2) pyridine / 1) 145 deg C, 3h, autoclave

3: 0.61 g / selenium dioxide / dimethylsulfoxide / 3h, 95 deg C, room temp. 2h

4: 1) sodium borohydride, 2) sodium hydroxide / 1)water, ethanol, 12h, roomtemp., 2) reflux, 4h

5: 0.35 g / sodium isobutyrate

6: 45 mg / m-chloroperbenzoic acid / CHCl₃ / 56 h / Ambient temperature

With pyridine; sodium hydroxide; sodium tetrahydroborate; selenium(IV) oxide; isobutyric acid sodium salt; 3-chloro-benzenecarboperoxoic acid; In chloroform; acetic acid; dimethyl sulfoxide;

Reference yield:

: 8,10-didehydro-7,9-dihydroxythymol

: 64190-69-8
2-hydroxymethyl-2-(2'-hydroxy-4'-hydroxymethylphenyl)oxirane triisobutyrate

Guidance literature:: Multi-step reaction with 2 steps

1: 0.35 g / sodium isobutyrate

2: 45 mg / m-chloroperbenzoic acid / CHCl₃ / 56 h / Ambient temperature

With isobutyric acid sodium salt; 3-chloro-benzenecarboperoxoic acid; In chloroform;