14-benzyloxy-16-methylbenzo-1,4,7,10,13-pentaoxacyclopentadecane

Base Information

Chemical Name:14-benzyloxy-16-methylbenzo-1,4,7,10,13-pentaoxacyclopentadecane
CAS No.:152898-04-9
Molecular Formula:C₂₂H₂₈O₆
Molecular Weight:388.461
Hs Code.:

Synonyms:

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Chemical Property of 14-benzyloxy-16-methylbenzo-1,4,7,10,13-pentaoxacyclopentadecane

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Technology Process of 14-benzyloxy-16-methylbenzo-1,4,7,10,13-pentaoxacyclopentadecane

There total 6 articles about 14-benzyloxy-16-methylbenzo-1,4,7,10,13-pentaoxacyclopentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6443-69-2
3,4,5-trimethoxytoluene

: 152898-04-9
14-benzyloxy-16-methylbenzo-1,4,7,10,13-pentaoxacyclopentadecane

Guidance literature:: Multi-step reaction with 5 steps

1: 96 percent / 57percent HI, 30percent aq. H₃PO₂ / Heating

2: 82 percent / molecular sieves 4 Angstroem / Amberlite IR 120-plus / benzene / Heating

3: K₂CO₃ / Bu₄NHSO₄ / acetone / 24 h / Heating

4: TsOH / methanol; H₂O / 16 h / Ambient temperature

5: 3.9 g / K₂CO₃ / acetone / 15 h / Heating

With 4 A molecular sieve; hydrogen iodide; hypophosphorous acid; potassium carbonate; toluene-4-sulfonic acid; Amberlite IR 120-plus; tetra(n-butyl)ammonium hydrogensulfate; In methanol; water; acetone; benzene;
DOI:10.1055/s-1993-25945

Reference yield:

: 609-25-6
5-methylpyrogallol

: 152898-04-9
14-benzyloxy-16-methylbenzo-1,4,7,10,13-pentaoxacyclopentadecane

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / molecular sieves 4 Angstroem / Amberlite IR 120-plus / benzene / Heating

2: K₂CO₃ / Bu₄NHSO₄ / acetone / 24 h / Heating

3: TsOH / methanol; H₂O / 16 h / Ambient temperature

4: 3.9 g / K₂CO₃ / acetone / 15 h / Heating

With 4 A molecular sieve; potassium carbonate; toluene-4-sulfonic acid; Amberlite IR 120-plus; tetra(n-butyl)ammonium hydrogensulfate; In methanol; water; acetone; benzene;
DOI:10.1055/s-1993-25945

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 152898-04-9
14-benzyloxy-16-methylbenzo-1,4,7,10,13-pentaoxacyclopentadecane

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / H₂ / 10percent Pd/C / acetic acid / 72 h / 30002.4 Torr / Ambient temperature

2: 96 percent / 57percent HI, 30percent aq. H₃PO₂ / Heating

3: 82 percent / molecular sieves 4 Angstroem / Amberlite IR 120-plus / benzene / Heating

4: K₂CO₃ / Bu₄NHSO₄ / acetone / 24 h / Heating

5: TsOH / methanol; H₂O / 16 h / Ambient temperature

6: 3.9 g / K₂CO₃ / acetone / 15 h / Heating

With 4 A molecular sieve; hydrogen iodide; hydrogen; hypophosphorous acid; potassium carbonate; toluene-4-sulfonic acid; palladium on activated charcoal; Amberlite IR 120-plus; tetra(n-butyl)ammonium hydrogensulfate; In methanol; water; acetic acid; acetone; benzene;
DOI:10.1055/s-1993-25945