2-o-chlorophenyl-6-mercaptobenzo-v-triazolo<4,5-h>benzo-as-triazine

Base Information

Chemical Name:2-o-chlorophenyl-6-mercaptobenzo-v-triazolo<4,5-h>benzo-as-triazine
CAS No.:118971-26-9
Molecular Formula:C₁₇H₉ClN₆S
Molecular Weight:364.818
Hs Code.:

2-o-chlorophenyl-6-mercaptobenzo<f>-v-triazolo<4,5-h>benzo<e>-as-triazine

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Chemical Property of 2-o-chlorophenyl-6-mercaptobenzo-v-triazolo<4,5-h>benzo-as-triazine

Chemical Property:

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Technology Process of 2-o-chlorophenyl-6-mercaptobenzo-v-triazolo<4,5-h>benzo-as-triazine

There total 5 articles about 2-o-chlorophenyl-6-mercaptobenzo-v-triazolo<4,5-h>benzo-as-triazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 118971-24-7
2-o-chlorophenyl-2H-naphtho<1,2-d>-v-triazole-4,5-quinone 4-monothiosemicarbazone

: 118971-26-9
2-o-chlorophenyl-6-mercaptobenzo-v-triazolo<4,5-h>benzo-as-triazine

Guidance literature:: With potassium hydroxide; for 0.5h; Heating;

Reference yield:

: 118971-21-4
2-o-chlorophenyl-2H-naphtho<1,2-d>-v-triazole-4,5-quinone

: 118971-26-9
2-o-chlorophenyl-6-mercaptobenzo-v-triazolo<4,5-h>benzo-as-triazine

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / acetic acid / 0.33 h / Heating

2: 47 percent / 5percent aq. KOH / 0.5 h / Heating

With potassium hydroxide; In acetic acid;

Reference yield:

: 95-51-2
o-chloroaniline

: 118971-26-9
2-o-chlorophenyl-6-mercaptobenzo-v-triazolo<4,5-h>benzo-as-triazine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.)NaNO₂/aq. HCl 2.)NaOAc / 1.)below 5 deg C 2.)EtOH, 40 deg C

2: 61 percent / CrO₃/Ac₂O / acetic acid

3: 54 percent / acetic acid / 0.33 h / Heating

4: 47 percent / 5percent aq. KOH / 0.5 h / Heating

With chromium(VI) oxide; hydrogenchloride; potassium hydroxide; sodium acetate; acetic anhydride; sodium nitrite; In acetic acid;