2-Chlor-N-methylthiobenzanilid

Base Information

• Chemical Name: 2-Chlor-N-methylthiobenzanilid
• CAS No.: 100363-25-5
• Molecular Formula: C₁₄H₁₂ClNS
• Molecular Weight: 261.775
• Mol file: 100363-25-5.mol

Synonyms:

Chemical Property of 2-Chlor-N-methylthiobenzanilid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Chlor-N-methylthiobenzanilid

There total 3 articles about 2-Chlor-N-methylthiobenzanilid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

o-chlorobenzoyl chloride (609-65-4) + N-methylaniline (100-61-8) → 2-Chlor-N-methylthiobenzanilid (100363-25-5)

Guidance literature:

With tetraphosphorus decasulfide; In pyridine;

Reference yield:

3-chloro-N-methyl-N-phenylbenzothioamide (69859-25-2) → 2-Chlor-N-methylthiobenzanilid (100363-25-5)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / electroreduction, Hg electrode

2: 67 percent / P₂S₅ / pyridine

With tetraphosphorus decasulfide; In pyridine; acetonitrile;

Reference yield:

N-methylthiobenzanilide (2628-58-2) → 2-Chlor-N-methylthiobenzanilid (100363-25-5)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile / electroreduction, Hg electrode

2: 67 percent / P₂S₅ / pyridine

With tetraphosphorus decasulfide; In pyridine; acetonitrile;

upstream raw materials:

o-chlorobenzoyl chloride

N-methylaniline

3-chloro-N-methyl-N-phenylbenzothioamide

N-methylthiobenzanilide

Downstream raw materials:

N-methylthiobenzanilide

2-chloro-N-methyl-N-phenylbenzylamine

Refernces