Ru(III)(CCPh)(dppe)Cp*

Base Information

Chemical Name:Ru(III)(CCPh)(dppe)Cp*
CAS No.:113152-57-1
Molecular Formula:C₄₄H₄₄P₂Ru
Molecular Weight:735.851
Hs Code.:

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Chemical Property of Ru(III)(CCPh)(dppe)Cp*

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Technology Process of Ru(III)(CCPh)(dppe)Cp*

There total 3 articles about Ru(III)(CCPh)(dppe)Cp* which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: phenylethynyl(triphenylphosphine)gold(I)

: pentamethylcyclopentadienyl(1,2-bis(diphenylphosphino)ethane)chlororuthenium(II)

: 113152-57-1
Ru(III)(CCPh)(dppe)Cp*

Guidance literature:: With NH₄PF₆; DBU; In methanol; under N2 atm. suspn. Ru complex, Au complex and NH4PF6 in MeOH was heated at reflux for 1 h, DBU was added and stirred for 1 h; ppt. was filtered, washed with cold MeOH and air-dried;
DOI:10.1039/b809960j

Reference yield: 40.0%

: pentamethylcyclopentadienyl(1,2-bis(diphenylphosphino)ethane)chlororuthenium(II)

: 536-74-3
phenylacetylene

: 113152-57-1
Ru(III)(CCPh)(dppe)Cp*

Guidance literature:: With sodium methylate; In methanol; soln. RuCl(dppe)(C5Me5) and HCCPh in MeOH refluxed with stirring for 1 h under N2, cooled, CH3ONa soln. added dropwise, stirred for 20 min; concd., ppt. washed with CH3OH, recrystd. (hexane, at -20°C), elem. anal.;
DOI:10.1016/0022-328X(87)85198-7