2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-7-O-<2,3,4,6-tetrakis-O-(phenylmethyl)-α-D-glucopyranosyl>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-hepitol

Base Information

Chemical Name:2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-7-O-<2,3,4,6-tetrakis-O-(phenylmethyl)-α-D-glucopyranosyl>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-hepitol
CAS No.:104419-28-5
Molecular Formula:C₇₇H₇₉NO₁₂
Molecular Weight:1210.47
Hs Code.:

2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-7-O-<2,3,4,6-tetrakis-O-(phenylmethyl)-α-D-glucopyranosyl>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-hepitol

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Chemical Property of 2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-7-O-<2,3,4,6-tetrakis-O-(phenylmethyl)-α-D-glucopyranosyl>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-hepitol

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Technology Process of 2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-7-O-<2,3,4,6-tetrakis-O-(phenylmethyl)-α-D-glucopyranosyl>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-hepitol

There total 3 articles about 2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-7-O-<2,3,4,6-tetrakis-O-(phenylmethyl)-α-D-glucopyranosyl>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-hepitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 104419-28-5
2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-7-O-<2,3,4,6-tetrakis-O-(phenylmethyl)-α-D-glucopyranosyl>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-hepitol

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / tetrahydrofuran / 1 h / Ambient temperature

3: 1.) HgBr₂, 4A molecular sieves / 1.) CH₂Cl₂, RT, 1 h, 2.) CH₂Cl₂, RT, overnight

With 4 A molecular sieve; potassium carbonate; mercury dibromide; In tetrahydrofuran;
DOI:10.1021/jo00230a012

Reference yield:

: 104343-30-8
1,2,6-trideoxy-6-<<(phenylmethoxy)carbonyl>amino>-3,4,5,7-tetrakis-O-(phenylmethyl)-D-gluco-hept-1-enitol

: 104419-28-5
2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-7-O-<2,3,4,6-tetrakis-O-(phenylmethyl)-α-D-glucopyranosyl>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-hepitol

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) HgBr₂, 4A molecular sieves / 1.) CH₂Cl₂, RT, 1 h, 2.) CH₂Cl₂, RT, overnight

With 4 A molecular sieve; mercury dibromide;
DOI:10.1021/jo00230a012

Reference yield:

: 4196-35-4
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl bromide

: 104343-31-9
2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-heptitol

: 104343-32-0
2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-7-O-<2,3,4,6-tetrakis-O-(phenylmethyl)-β-D-glucopyranosyl>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-hepitol

: 104419-28-5
2,6-dideoxy-2,6-<<(phenylmethoxy)carbonyl>imino>-7-O-<2,3,4,6-tetrakis-O-(phenylmethyl)-α-D-glucopyranosyl>-1,3,4,5-tetrakis-O-(phenylmethyl)-D-glycero-L-gulo-hepitol

Guidance literature:: With 4 A molecular sieve; mercury dibromide; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, RT, 1 h, 2.) CH₂Cl₂, RT, overnight;
DOI:10.1021/jo00230a012