3-Phenyl-7H-cyclohepta-1,2,4-triazin-7-on-oxim

Base Information

Chemical Name:3-Phenyl-7H-cyclohepta-1,2,4-triazin-7-on-oxim
CAS No.:344763-55-9
Molecular Formula:C₁₄H₁₀N₄O
Molecular Weight:250.26
Hs Code.:

3-Phenyl-7H-cyclohepta<e>-1,2,4-triazin-7-on-oxim

Synonyms:

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Chemical Property of 3-Phenyl-7H-cyclohepta-1,2,4-triazin-7-on-oxim

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Technology Process of 3-Phenyl-7H-cyclohepta-1,2,4-triazin-7-on-oxim

There total 4 articles about 3-Phenyl-7H-cyclohepta-1,2,4-triazin-7-on-oxim which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 88396-02-5
3-Phenyl-7H-cyclohepta-1,2,4-triazin-7-on

: 344763-55-9
3-Phenyl-7H-cyclohepta-1,2,4-triazin-7-on-oxim

Guidance literature:: With sodium hydroxide; hydroxylamine hydrochloride; In ethanol; water; for 0.833333h; Heating;

Reference yield: 52.0%

: 5-Nitrosotropolon

: 28819-30-9
benzamidrazone

: 344763-55-9
3-Phenyl-7H-cyclohepta-1,2,4-triazin-7-on-oxim

Guidance literature:: In methanol; ethyl acetate; at 40 ℃; for 96h;

Reference yield:

: 56561-57-0
3,6-Cycloheptadien-1,2,5-trion

: 344763-55-9
3-Phenyl-7H-cyclohepta-1,2,4-triazin-7-on-oxim

Guidance literature:: Multi-step reaction with 2 steps

1: 53 percent / CHCl₃; methanol / 1) 15 min, room temperature, 2) 12 h, reflux

2: 70 percent / NH₂OH*HCl, 10percent NaOH / H₂O; ethanol / 0.83 h / Heating

With sodium hydroxide; hydroxylamine hydrochloride; In methanol; ethanol; chloroform; water;