Technology Process of C30H38N4O10
There total 7 articles about C30H38N4O10 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 1.) NaH / 1.) THF, room temp., 1 h, 2.) room temp., 40 h
2: 1.) NaH / 1.) THF, room temp., 1 h, 2.) THF, reflux, 18 h
3: 61 percent / TsOH, H2 / Pd/C / dioxane / Ambient temperature
4: 47 percent / NaH, KBF4 / tetrahydrofuran / 96 h / Heating
5: 80 percent / LiAlH4 / tetrahydrofuran / 15 h / Heating
6: 90 percent / CAN / acetonitrile / 1.5 h / Ambient temperature
7: 81 percent / conc. H2SO4 / ethanol / 1.5 h / Ambient temperature
With
lithium aluminium tetrahydride; ammonium cerium(IV) nitrate; sulfuric acid; hydrogen; sodium hydride; toluene-4-sulfonic acid; potassium tetrafluoroborate;
palladium on activated charcoal;
In
tetrahydrofuran; 1,4-dioxane; ethanol; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) NaH / 1.) THF, room temp., 1 h, 2.) THF, reflux, 18 h
2: 61 percent / TsOH, H2 / Pd/C / dioxane / Ambient temperature
3: 47 percent / NaH, KBF4 / tetrahydrofuran / 96 h / Heating
4: 80 percent / LiAlH4 / tetrahydrofuran / 15 h / Heating
5: 90 percent / CAN / acetonitrile / 1.5 h / Ambient temperature
6: 81 percent / conc. H2SO4 / ethanol / 1.5 h / Ambient temperature
With
lithium aluminium tetrahydride; ammonium cerium(IV) nitrate; sulfuric acid; hydrogen; sodium hydride; toluene-4-sulfonic acid; potassium tetrafluoroborate;
palladium on activated charcoal;
In
tetrahydrofuran; 1,4-dioxane; ethanol; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: diisopropyl ether / 50 h / Ambient temperature; lipase YS
2: 1.) NaH / 1.) THF, room temp., 1 h, 2.) THF, reflux, 18 h
3: 61 percent / TsOH, H2 / Pd/C / dioxane / Ambient temperature
4: 47 percent / NaH, KBF4 / tetrahydrofuran / 96 h / Heating
5: 80 percent / LiAlH4 / tetrahydrofuran / 15 h / Heating
6: 90 percent / CAN / acetonitrile / 1.5 h / Ambient temperature
7: 81 percent / conc. H2SO4 / ethanol / 1.5 h / Ambient temperature
With
lithium aluminium tetrahydride; ammonium cerium(IV) nitrate; sulfuric acid; hydrogen; sodium hydride; toluene-4-sulfonic acid; potassium tetrafluoroborate;
palladium on activated charcoal;
In
tetrahydrofuran; 1,4-dioxane; ethanol; di-isopropyl ether; acetonitrile;