[((C₅H₅)ClTi)2Cl₂(NNC(C₆H₅)2)]*C₄H₈O

Base Information

• Chemical Name: [((C₅H₅)ClTi)2Cl₂(NNC(C₆H₅)2)]*C₄H₈O
• CAS No.: 87587-74-4
• Molecular Formula: C₄H₈O*C₂₃H₂₀Cl₄N₂Ti₂
• Molecular Weight: 634.104

Synonyms:

Chemical Property of [((C₅H₅)ClTi)2Cl₂(NNC(C₆H₅)2)]*C₄H₈O

Chemical Property:

Purity/Quality:

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Technology Process of [((C₅H₅)ClTi)2Cl₂(NNC(C₆H₅)2)]*C₄H₈O

There total 1 articles about [((C₅H₅)ClTi)2Cl₂(NNC(C₆H₅)2)]*C₄H₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[(cyclopentadienyl)-di(chloro)-titanium(III)]n + diazodiphenylmethane (908093-98-1) → [((C5H5)ClTi)2Cl2(NNC(C6H5)2)]*C4H8O (87587-74-4) + (TiCl(C5H5))2(N2C(C6H5)2)2

Guidance literature:

With C₄H₈O; In tetrahydrofuran; soln. of CpTiCl2 in THF reacted with neat Ph2CN2 under N2; ppt. of ((CpTiCl)2Cl2(NNCPh))*THF filtered, to filtrate added Et2O, in few hs ppt. of ((CpClTi)2(NNCPh2)2) formed; elem. anal.;

DOI:10.1021/ja00363a015

Reference yield:

[((C5H5)ClTi)2Cl2(NNC(C6H5)2)]*C4H8O (87587-74-4) → cyclopentadienyl titanium(IV) trichloride (1270-98-0) + (TiCl(C5H5))2(N2C(C6H5)2)2

Guidance literature:

In tetrahydrofuran; refluxed for few min under N2; (CpTiCl)2(NNCPh2)2 crystd. by addn. of Et2O, filtered soln. evapd., residue collected with toluene and heated, suspn. filtered when hot, added hexane, CpTiCl3 crystd. from this soln.;

DOI:10.1021/ja00363a015

upstream raw materials:

diazodiphenylmethane

Downstream raw materials:

cyclopentadienyl titanium(IV) trichloride

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