Technology Process of 8-amino pentacyclo<5.4.0.02,6.03,10.05,9>undecane hydrochloride
There total 8 articles about 8-amino pentacyclo<5.4.0.02,6.03,10.05,9>undecane hydrochloride which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium hydroxide / 190 °C
2: chromium(VI) oxide; acetic acid / water / 90 °C
3: hydroxylamine hydrochloride; sodium acetate
4: lithium aluminium tetrahydride
With
chromium(VI) oxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; sodium acetate; acetic acid; potassium hydroxide;
In
water;
DOI:10.1021/ml100297w
- Guidance literature:
-
Multi-step reaction with 3 steps
1: chromium(VI) oxide; acetic acid / water / 90 °C
2: hydroxylamine hydrochloride; sodium acetate
3: lithium aluminium tetrahydride
With
chromium(VI) oxide; lithium aluminium tetrahydride; hydroxylamine hydrochloride; sodium acetate; acetic acid;
In
water;
DOI:10.1021/ml100297w
- Guidance literature:
-
Multi-step reaction with 8 steps
1: toluene-4-sulfonic acid / benzene / Reflux
2: sodium tetrahydroborate / ethanol
3: hydrogenchloride / methanol
4: hydrazine / diethylene glycol / 120 °C
5: potassium hydroxide / 190 °C
6: chromium(VI) oxide; acetic acid / water / 90 °C
7: hydroxylamine hydrochloride; sodium acetate
8: lithium aluminium tetrahydride
With
chromium(VI) oxide; hydrogenchloride; sodium tetrahydroborate; lithium aluminium tetrahydride; hydroxylamine hydrochloride; sodium acetate; toluene-4-sulfonic acid; acetic acid; potassium hydroxide; hydrazine;
In
methanol; ethanol; water; diethylene glycol; benzene;
DOI:10.1021/ml100297w
