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Technology Process of C20H23NO3

C20H23NO3

Base Information
  • Chemical Name:C20H23NO3
  • CAS No.:1253912-59-2
  • Molecular Formula:C20H23NO3
  • Molecular Weight:325.408
  • Hs Code.:
C<sub>20</sub>H<sub>23</sub>NO<sub>3</sub>

Synonyms:

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Chemical Property of C20H23NO3
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Technology Process of C20H23NO3

There total 5 articles about C20H23NO3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C<sub>15</sub>H<sub>14</sub>O<sub>2</sub>

C15H14O2

C<sub>20</sub>H<sub>23</sub>NO<sub>3</sub>
1253912-59-2

C20H23NO3

Guidance literature:
Multi-step reaction with 3 steps
1: sodium azide; lithium perchlorate / acetonitrile
2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C / 760.05 Torr
3: di-isopropyl azodicarboxylate; triphenylphosphine / chloroform / Reflux
With sodium azide; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; lithium perchlorate; triphenylphosphine; In chloroform; ethyl acetate; acetonitrile;
DOI:10.1002/cmdc.201000109

Reference yield:

C<sub>15</sub>H<sub>15</sub>N<sub>3</sub>O<sub>2</sub>

C15H15N3O2

C<sub>20</sub>H<sub>23</sub>NO<sub>3</sub>
1253912-59-2

C20H23NO3

Guidance literature:
Multi-step reaction with 2 steps
1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C / 760.05 Torr
2: di-isopropyl azodicarboxylate; triphenylphosphine / chloroform / Reflux
With di-isopropyl azodicarboxylate; palladium 10% on activated carbon; hydrogen; triphenylphosphine; In chloroform; ethyl acetate;
DOI:10.1002/cmdc.201000109

Reference yield:

C<sub>20</sub>H<sub>25</sub>NO<sub>4</sub>

C20H25NO4

C<sub>20</sub>H<sub>23</sub>NO<sub>3</sub>
1253912-59-2

C20H23NO3

Guidance literature:
With di-isopropyl azodicarboxylate; triphenylphosphine; In chloroform; Reflux;
DOI:10.1002/cmdc.201000109
upstream raw materials:

di-tert-butyl dicarbonate

(E)-3-([1,1'-biphenyl]-4-yl)prop-2-en-1-ol

Downstream raw materials:

(3R,E)-3-amino-3-(4'-biphenyl)-1-phenylsulfonyl-1-propene trifluoroacetate salt

N-((S)-1-((R,E)-1-(biphenyl-4-yl)-3-(phenylsulfonyl)allylamino)-1-oxo-3-phenylpropan-2-yl)morpholine-4-carboxamide

N-((S)-1-((R,E)-1-(biphenyl-4-yl)-3-(phenylsulfonyl)allylamino)-4-methyl-1-oxopentan-2-yl)morpholine-4-carboxamide

N-((S)-1-((R,E)-1-(biphenyl-4-yl)-3-(phenylsulfonyl)allylamino)-1-oxo-3-phenylpropan-2-yl)-4-methylpiperazine-1-carboxamide

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