BOC-D-PheΨProOH*CF3COOH

Base Information

Chemical Name:BOC-D-PheΨProOH*CF3COOH
CAS No.:133773-52-1
Molecular Formula:C₂HF₃O₂*C₁₉H₂₈N₂O₄
Molecular Weight:462.466
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of BOC-D-PheΨProOH*CF3COOH

Chemical Property:

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Technology Process of BOC-D-PheΨProOH*CF3COOH

There total 3 articles about BOC-D-PheΨProOH*CF3COOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 133773-52-1
BOC-D-PheΨProOH*CF3COOH

Guidance literature:: Multi-step reaction with 3 steps

1: NEt₃, (benzotriazolyloxy)tris(dimethylamino)phosphonium hexafluorophosphate (BOP) / acetonitrile / 1 h / Ambient temperature

2: 29.6 percent / B₂H₆ / tetrahydrofuran / 24 h / Ambient temperature

3: 1.) aq. 1 N NaOH / 1.) MeOH, 6 h, room tempertaure, 2.) CH₃CN

With sodium hydroxide; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; diborane; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jo00013a017

Reference yield:

: 126251-09-0
Boc-D-Phe-L-Pro-OMe

: 133773-52-1
BOC-D-PheΨProOH*CF3COOH

Guidance literature:: Multi-step reaction with 2 steps

1: 29.6 percent / B₂H₆ / tetrahydrofuran / 24 h / Ambient temperature

2: 1.) aq. 1 N NaOH / 1.) MeOH, 6 h, room tempertaure, 2.) CH₃CN

With sodium hydroxide; diborane; In tetrahydrofuran;
DOI:10.1021/jo00013a017

Reference yield:

: 118447-07-7
BOC-D-PheΨProOMe

: 76-05-1
trifluoroacetic acid

: 133773-52-1
BOC-D-PheΨProOH*CF3COOH

Guidance literature:: With sodium hydroxide; Yield given. Multistep reaction; 1.) MeOH, 6 h, room tempertaure, 2.) CH₃CN;
DOI:10.1021/jo00013a017