C₃₃H₃₅O₅SiN₃

Base Information

Chemical Name:C₃₃H₃₅O₅SiN₃
CAS No.:919076-85-0
Molecular Formula:C₃₃H₃₅N₃O₅Si
Molecular Weight:581.744
Hs Code.:

C<sub>33</sub>H<sub>35</sub>O<sub>5</sub>SiN<sub>3</sub>

Synonyms:

Suppliers and Price of C₃₃H₃₅O₅SiN₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₃H₃₅O₅SiN₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₃H₃₅O₅SiN₃

There total 11 articles about C₃₃H₃₅O₅SiN₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 919076-84-9
N-(1-{(2R,5R)-5-[(2,2-dimethyl-1,1-diphenyl-1-silapropoxy)methyl]-5-(hydroxymethyl)oxolan-2-yl}-2-oxohydropyrimidin-4-yl)benzamide

: 919076-85-0
C₃₃H₃₅O₅SiN₃

Guidance literature:: With dichloro-acetic acid; dicyclohexyl-carbodiimide; In dimethyl sulfoxide; at 0 ℃; for 2h;
DOI:10.1016/j.bmc.2006.09.061

Reference yield:

: 919076-88-3
(R)-5-[(2,2-dimethyl-1,1-diphenyl-1-silapropoxy)methyl]-5-[(phenylmethoxy)methyl]-3,4,5-trihydrofuran-2-one

: 919076-85-0
C₃₃H₃₅O₅SiN₃

Guidance literature:: Multi-step reaction with 7 steps

1: 91.2 percent / diisobutylaluminum hydride / toluene; hexane / 1 h / -78 °C

2: 98 percent / pyridine / 24 h / 20 °C

3: 92.9 percent / HCOOH / Pd / methanol / 2.5 h

4: 97.1 percent / pyridine / 24 h / 20 °C

5: 0.525 g / trimethylsilyl triflate / 1,2-dichloro-ethane / 2.5 h / cooling

6: 87.5 percent / guanidine / ethanol; CH₂Cl₂ / 0.5 h / 0 - 20 °C

7: dicyclohexylcarbodiimide; dichloroacetic acid / dimethylsulfoxide / 2 h / 0 °C

With pyridine; dichloro-acetic acid; formic acid; trimethylsilyl trifluoromethanesulfonate; diisobutylaluminium hydride; guanidine nitrate; dicyclohexyl-carbodiimide; palladium; In methanol; ethanol; hexane; dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane; toluene;
DOI:10.1016/j.bmc.2006.09.061

Reference yield:

: 919076-89-4
5-[(2,2-dimethyl-1,1-diphenyl-1-silapropoxy)methyl]-5-[(phenylmethoxy)methyl]oxolan-2-ol

: 919076-85-0
C₃₃H₃₅O₅SiN₃

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / pyridine / 24 h / 20 °C

2: 92.9 percent / HCOOH / Pd / methanol / 2.5 h

3: 97.1 percent / pyridine / 24 h / 20 °C

4: 0.525 g / trimethylsilyl triflate / 1,2-dichloro-ethane / 2.5 h / cooling

5: 87.5 percent / guanidine / ethanol; CH₂Cl₂ / 0.5 h / 0 - 20 °C

6: dicyclohexylcarbodiimide; dichloroacetic acid / dimethylsulfoxide / 2 h / 0 °C

With pyridine; dichloro-acetic acid; formic acid; trimethylsilyl trifluoromethanesulfonate; guanidine nitrate; dicyclohexyl-carbodiimide; palladium; In methanol; ethanol; dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane;
DOI:10.1016/j.bmc.2006.09.061