trans-hydroxo(4-nitrophenyl phosphato)bis(1,2-ethanediamine)cobalt(III)

Base Information

• Chemical Name: trans-hydroxo(4-nitrophenyl phosphato)bis(1,2-ethanediamine)cobalt(III)
• CAS No.: 87183-66-2
• Molecular Formula: C₁₀H₂₁CoN₅O₇P
• Molecular Weight: 413.273

Synonyms:

Chemical Property of trans-hydroxo(4-nitrophenyl phosphato)bis(1,2-ethanediamine)cobalt(III)

Chemical Property:

Purity/Quality:

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Technology Process of trans-hydroxo(4-nitrophenyl phosphato)bis(1,2-ethanediamine)cobalt(III)

There total 4 articles about trans-hydroxo(4-nitrophenyl phosphato)bis(1,2-ethanediamine)cobalt(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

rac-bis(μ-4-nitrophenyl phosphato)bis[bis(1,2-ethanediamine)cobalt(III)] → 4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + {Co(ethylenediamine)2(OH)2}(1+) + trans-hydroxo(4-nitrophenyl phosphato)bis(1,2-ethanediamine)cobalt(III) (87183-66-2,93060-62-9) + cis-hydroxo(4-nitrophenyl phosphato)bis(1,2-ethanediamine)cobalt(III) + [(HO)(NH2(CH2)2NH2)2Co(PO4)Co(NH2(CH2)2NH2)2(O3POC6H4NO2)] (93000-36-3)

Guidance literature:

With NaOH; In water; water-d2; temp. of soln. of educt in H2O/D2O adjusted to 25°C, soln. of NaOH added rapidly to 0.5 M concn. of OH(1-) / further products; not isolated; monitored by NMR;

DOI:10.1021/ja00337a026

Reference yield:

meso-bis(μ-4-nitrophenyl phosphato)bis[bis(1,2-ethanediamine)cobalt(III)] (93060-59-4,93060-60-7,93060-68-5) → mono-p-nitrophenyl phosphate (330-13-2) + trans-hydroxo(4-nitrophenyl phosphato)bis(1,2-ethanediamine)cobalt(III) (87183-66-2,93060-62-9) + cis-hydroxo(4-nitrophenyl phosphato)bis(1,2-ethanediamine)cobalt(III) + [(HO)(NH2(CH2)2NH2)2Co(PO4)Co(NH2(CH2)2NH2)2(O3POC6H4NO2)] (93000-36-3)

Guidance literature:

With NaOH; In water; water-d2; temp. of soln. of educt in H2O/D2O adjusted to 5.+-.1°C, soln. of NaOH added rapidly to 0.2 M concn. of OH(1-), reacted for 1210 s; not isolated; monitored by NMR; Kinetics;

DOI:10.1021/ja00337a026

Reference yield:

rac-bis(μ-4-nitrophenyl phosphato)bis[bis(1,2-ethanediamine)cobalt(III)] → mono-p-nitrophenyl phosphate (330-13-2) + trans-hydroxo(4-nitrophenyl phosphato)bis(1,2-ethanediamine)cobalt(III) (87183-66-2,93060-62-9) + cis-hydroxo(4-nitrophenyl phosphato)bis(1,2-ethanediamine)cobalt(III) + [(HO)(NH2(CH2)2NH2)2Co(PO4)Co(NH2(CH2)2NH2)2(O3POC6H4NO2)] (93000-36-3)

Guidance literature:

With NaOH; In water; water-d2; temp. of soln. of educt in H2O/D2O adjusted to 5.+-.1°C, soln. of NaOH added rapidly to 0.2 M concn. of OH(1-), reacted for 1305 s; not isolated; monitored by NMR;

DOI:10.1021/ja00337a026

upstream raw materials:

meso-bis(μ-4-nitrophenyl phosphato)bis[bis(1,2-ethanediamine)cobalt(III)]

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