Technology Process of C18H19N7O2
There total 5 articles about C18H19N7O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
1,4-dioxane;
at 0 - 20 ℃;
for 20h;
Inert atmosphere;
DOI:10.1002/cmdc.201100265
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N,N-dimethyl-formamide / 24 h / 170 °C / Inert atmosphere
2: hydroxylamine hydrochloride; potassium carbonate / ethanol / 20 - 90 °C / Inert atmosphere
3: sodium hydroxide / 1,4-dioxane / 20 h / 0 - 20 °C / Inert atmosphere
With
hydroxylamine hydrochloride; potassium carbonate; sodium hydroxide;
In
1,4-dioxane; ethanol; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201100265
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper(ll) sulfate pentahydrate; sodium carbonate; L-proline; ascorbic acid / water; dimethyl sulfoxide / 65 °C / Inert atmosphere
2: N,N-dimethyl-formamide / 24 h / 170 °C / Inert atmosphere
3: hydroxylamine hydrochloride; potassium carbonate / ethanol / 20 - 90 °C / Inert atmosphere
4: sodium hydroxide / 1,4-dioxane / 20 h / 0 - 20 °C / Inert atmosphere
With
copper(ll) sulfate pentahydrate; hydroxylamine hydrochloride; sodium carbonate; potassium carbonate; L-proline; sodium hydroxide; ascorbic acid;
In
1,4-dioxane; ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201100265
