Mn(C₆H₅CH₂NCH(C₆H₃)(NO₂)(O))2Cl

Base Information

Chemical Name:Mn(C₆H₅CH₂NCH(C₆H₃)(NO₂)(O))2Cl
CAS No.:101019-91-4
Molecular Formula:C₂₈H₂₂ClMnN₄O₆
Molecular Weight:600.897
Hs Code.:

Mn(C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>NCH(C<sub>6</sub>H<sub>3</sub>)(NO<sub>2</sub>)(O))2Cl

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Chemical Property of Mn(C₆H₅CH₂NCH(C₆H₃)(NO₂)(O))2Cl

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Technology Process of Mn(C₆H₅CH₂NCH(C₆H₃)(NO₂)(O))2Cl

There total 1 articles about Mn(C₆H₅CH₂NCH(C₆H₃)(NO₂)(O))2Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19513-05-4
manganese(III) triacetate dihydrate

: 88373-80-2
N-benzyl-3-nitro-salicylaldimine

: 101019-91-4
Mn(C₆H₅CH₂NCH(C₆H₃)(NO₂)(O))2Cl

Guidance literature:: With lithium chloride; In methanol; dichloromethane; soln. of Mn salt, ligand and LiCl in methanol-CH2Cl2 was refluxed for 1h; solvents were removed in vac., ppt. was recrystd. from CH2Cl2-ether, washed with 2-propanol, dried in vac.;
DOI:10.1016/S0277-5387(00)86708-X

Reference yield:

: 101019-91-4
Mn(C₆H₅CH₂NCH(C₆H₃)(NO₂)(O))2Cl

: 77997-95-6
Mn(C₆H₅CH₂NCH(C₆H₃)(NO₂)(O))2Cl₂

Guidance literature:: With hydrogen chloride; In isopropyl alcohol; soln. of HCl was added dropwise (1.5 excess) to soln. of Mn complex at 25°C and stirred for 30 min; ppt. was filtered off, washed with 2-propanol and ether, dried in vac.,elem. anal.;
DOI:10.1016/S0277-5387(00)86708-X

Reference yield:

: 101019-91-4
Mn(C₆H₅CH₂NCH(C₆H₃)(NO₂)(O))2Cl

: Mn(C₆H₅CH₂NCH(C₆H₃)(NO₂)(O))2(H₂O)2

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen chloride / isopropyl alcohol

2: water / isopropyl alcohol

With hydrogen chloride; water; In isopropyl alcohol;
DOI:10.1016/S0277-5387(00)86708-X