[Rh(1,3-bis(diphenylphosphino)propane)(CO)I]

Base Information

Chemical Name:[Rh(1,3-bis(diphenylphosphino)propane)(CO)I]
CAS No.:122924-41-8
Molecular Formula:C₂₈H₂₆IOP₂Rh
Molecular Weight:670.271
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Rh(1,3-bis(diphenylphosphino)propane)(CO)I]

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Technology Process of [Rh(1,3-bis(diphenylphosphino)propane)(CO)I]

There total 1 articles about [Rh(1,3-bis(diphenylphosphino)propane)(CO)I] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1254729-92-4
[Rh(1,3-bis(diphenylphosphino)propane)(COCF₃)I₂]

: 122924-41-8
[Rh(1,3-bis(diphenylphosphino)propane)(CO)I]

Guidance literature:: With K₂(benzophenone) or K(benzophenone); In tetrahydrofuran; tetrahydrofuran-d8; (N2); glovebox; soln. of Rh complex in THF-d8 was treated with soln. of K salt in THF; NMR mmonitoring;
DOI:10.1021/om1007055

Reference yield: 78.0%

: 122924-41-8
[Rh(1,3-bis(diphenylphosphino)propane)(CO)I]

: 407-25-0
trifluoroacetic anhydride

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

: 1254729-92-4
[Rh(1,3-bis(diphenylphosphino)propane)(COCF₃)I₂]

Guidance literature:: In toluene; (N2); glovebox; mixt. of Rh complex and anhydride in toluene was stirredfor 3 h; NaI was added; stirred for 4 h; hexane added; cooled in freezer for 0.5 h; filtered; washed (hexane); dissolved in CH2Cl2; filtered; concd. (vac.); hexane added; filtered; washed (hexane); dried in vac. at room temp. overnight; elem. anal.;
DOI:10.1021/om1007055