4,7-Bis-(toluene-4-sulfonyl)-[1,4,7]thiadiazecane

Base Information

Chemical Name:4,7-Bis-(toluene-4-sulfonyl)-[1,4,7]thiadiazecane
CAS No.:183242-98-0
Molecular Formula:C₂₁H₂₈N₂O₄S₃
Molecular Weight:468.662
Hs Code.:

Synonyms:

Suppliers and Price of 4,7-Bis-(toluene-4-sulfonyl)-[1,4,7]thiadiazecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,7-Bis-(toluene-4-sulfonyl)-[1,4,7]thiadiazecane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,7-Bis-(toluene-4-sulfonyl)-[1,4,7]thiadiazecane

There total 3 articles about 4,7-Bis-(toluene-4-sulfonyl)-[1,4,7]thiadiazecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56973-49-0
2-aminoethyl-3-aminopropyl sulfide

: 183242-98-0
4,7-Bis-(toluene-4-sulfonyl)-[1,4,7]thiadiazecane

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NaOH / H₂O; diethyl ether / 6 h / Ambient temperature

2: 1.) NaH (55-65 percent in oil) / 1.) DMF, r.t., 1.5 h, 70 deg C, 1.5 h; 2.) DMF, 105 deg C, 3 h

With sodium hydroxide; sodium hydride; In diethyl ether; water;
DOI:10.3891/acta.chem.scand.50-0853

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 183242-98-0
4,7-Bis-(toluene-4-sulfonyl)-[1,4,7]thiadiazecane

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NaOH / H₂O; diethyl ether / 6 h / Ambient temperature

2: 1.) NaH (55-65 percent in oil) / 1.) DMF, r.t., 1.5 h, 70 deg C, 1.5 h; 2.) DMF, 105 deg C, 3 h

With sodium hydroxide; sodium hydride; In diethyl ether; water;
DOI:10.3891/acta.chem.scand.50-0853

Reference yield:

: 6315-52-2
1,2-bis-tosyloxyethane

: 183242-97-9
N,N'-di(p-toluenesulfonyl)-2-aminoethyl-3-aminopropylsulfide

: 183242-98-0
4,7-Bis-(toluene-4-sulfonyl)-[1,4,7]thiadiazecane

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) DMF, r.t., 1.5 h, 70 deg C, 1.5 h; 2.) DMF, 105 deg C, 3 h;
DOI:10.3891/acta.chem.scand.50-0853