Technology Process of C7(2)H10O2(13)C
There total 8 articles about C7(2)H10O2(13)C which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: N-bromosuccinimide / CCl4 / Irradiation
2: 79 percent / 18-crown-6 / acetonitrile / 4 h / Heating
3: 80 percent / Na; deuterium oxide / 3 h / Heating
4: 91 percent / deuterium bromide / 0.08 h / 150 °C / microwave irradiation
5: 91 percent / DIEA / acetonitrile / microwave irradiation
6: lithium aluminum deuteride / diethyl ether
7: deuterium oxide; deuterium chloride
With
N-Bromosuccinimide; lithium aluminium deuteride; 18-crown-6 ether; water-d2; sodium; hydrogen chloride; deuterium bromide; N-ethyl-N,N-diisopropylamine;
In
tetrachloromethane; diethyl ether; acetonitrile;
DOI:10.1002/jlcr.1404
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 79 percent / 18-crown-6 / acetonitrile / 4 h / Heating
2: 80 percent / Na; deuterium oxide / 3 h / Heating
3: 91 percent / deuterium bromide / 0.08 h / 150 °C / microwave irradiation
4: 91 percent / DIEA / acetonitrile / microwave irradiation
5: lithium aluminum deuteride / diethyl ether
6: deuterium oxide; deuterium chloride
With
lithium aluminium deuteride; 18-crown-6 ether; water-d2; sodium; hydrogen chloride; deuterium bromide; N-ethyl-N,N-diisopropylamine;
In
diethyl ether; acetonitrile;
DOI:10.1002/jlcr.1404
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / Na; deuterium oxide / 3 h / Heating
2: 91 percent / deuterium bromide / 0.08 h / 150 °C / microwave irradiation
3: 91 percent / DIEA / acetonitrile / microwave irradiation
4: lithium aluminum deuteride / diethyl ether
5: deuterium oxide; deuterium chloride
With
lithium aluminium deuteride; water-d2; sodium; hydrogen chloride; deuterium bromide; N-ethyl-N,N-diisopropylamine;
In
diethyl ether; acetonitrile;
DOI:10.1002/jlcr.1404