Ta(OSi(C(CH₃)3)3)2(CH₂C₆H₅)Cl₂

Base Information

Chemical Name:Ta(OSi(C(CH₃)3)3)2(CH₂C₆H₅)Cl₂
CAS No.:97749-48-9
Molecular Formula:C₃₁H₆₁Cl₂O₂Si₂Ta
Molecular Weight:773.849
Hs Code.:

Ta(OSi(C(CH<sub>3</sub>)3)3)2(CH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)Cl<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ta(OSi(C(CH₃)3)3)2(CH₂C₆H₅)Cl₂

Chemical Property:

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Technology Process of Ta(OSi(C(CH₃)3)3)2(CH₂C₆H₅)Cl₂

There total 3 articles about Ta(OSi(C(CH₃)3)3)2(CH₂C₆H₅)Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 97733-17-0,148812-60-6
[(Me₃C)3SiO]2TaCl₃

: 6921-34-2
benzylmagnesium chloride

: 97749-48-9
Ta(OSi(C(CH₃)3)3)2(CH₂C₆H₅)Cl₂

Guidance literature:: In tetrahydrofuran; diethyl ether; an excess of Grignard reagent in THF adding to a soln. of Ta deriv. in Et2O at -78°C, warming to room temp., stirring for 20 h, solvent removing, hexane adding by distillation, solid filtering off, filtrate concg., cooling to -78°C; identified by elem. anal. and NMR spectra;
DOI:10.1021/om00129a022

Reference yield: 37.0%

: 97733-17-0,148812-60-6
[(Me₃C)3SiO]2TaCl₃

: 1589-82-8
phenylmagnesium bromide

: 97749-48-9
Ta(OSi(C(CH₃)3)3)2(CH₂C₆H₅)Cl₂

Guidance literature:: In diethyl ether;
DOI:10.1021/om00129a022

Reference yield:

: 97733-16-9
Na(silox)

: 97749-48-9
Ta(OSi(C(CH₃)3)3)2(CH₂C₆H₅)Cl₂

Guidance literature:: Multi-step reaction with 2 steps

1: toluene

2: tetrahydrofuran; diethyl ether

In tetrahydrofuran; diethyl ether; toluene;
DOI:10.1021/om00129a022