(C₆H₅CHCH)2Tl⁽¹⁺⁾*Br^(1-)=(C₆H₅CHCH)2TlBr

Base Information

• Chemical Name: (C₆H₅CHCH)2Tl⁽¹⁺⁾*Br^(1-)=(C₆H₅CHCH)2TlBr
• CAS No.: 87796-11-0
• Molecular Formula: Br*C₁₆H₁₄Tl
• Molecular Weight: 490.574

Synonyms:

Chemical Property of (C₆H₅CHCH)2Tl⁽¹⁺⁾*Br^(1-)=(C₆H₅CHCH)2TlBr

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of (C₆H₅CHCH)2Tl⁽¹⁺⁾*Br^(1-)=(C₆H₅CHCH)2TlBr

There total 1 articles about (C₆H₅CHCH)2Tl⁽¹⁺⁾*Br^(1-)=(C₆H₅CHCH)2TlBr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thallium(I) bromide + bromostyrene (103-64-0,1340-14-3) → (C6H5CHCH)2Tl(1+)*Br(1-)=(C6H5CHCH)2TlBr (87796-11-0)

Guidance literature:

With bromine; lithium; In tetrahydrofuran; diethyl ether; TlBr3 in THF (prepd. by mixing TlBr and Br2 in 1:1 ratio) was added at 0°C under Ar with vigorous stirring over 1 h to a soln. of PhCH=CHLi (prepd. from PhCH=CHBr (ca. 85% trans-isomer) and Li in Et2O at -5°C), mixt. was stirred for 20 min; filtered, ppt. was washed with water and Et2O and recrystd. from pyridine; elem. anal.;

DOI:10.1016/0022-328X(83)80054-0

Reference yield:

(C6H5CHCH)2Tl(1+)*Br(1-)=(C6H5CHCH)2TlBr (87796-11-0) + silver nitrate → (C6H5CHCH)2Tl(1+)*NO3(1-)=(C6H5CHCH)2TlNO3 (87795-97-9)

Guidance literature:

In methanol; byproducts: AgBr; stoich. amts. of (trans-PhCH=CH)2TlBr and AgNO3 were stirred together in methanol for several hours under Ar; AgBr was removed by filtration, filtrate evapd. at room temp., residue recrystd. from methanol; elem. anal.;

DOI:10.1016/0022-328X(83)80054-0

upstream raw materials:

bromostyrene

Downstream raw materials:

(C₆H₅CHCH)2Tl⁽¹⁺⁾*NO₃^(1-)=(C₆H₅CHCH)2TlNO₃

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