1-methyl 4-trichloroethyl itaconate

Base Information

Chemical Name:1-methyl 4-trichloroethyl itaconate
CAS No.:102651-57-0
Molecular Formula:C₈H₉Cl₃O₄
Molecular Weight:275.516
Hs Code.:

Synonyms:

Suppliers and Price of 1-methyl 4-trichloroethyl itaconate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-methyl 4-trichloroethyl itaconate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-methyl 4-trichloroethyl itaconate

There total 2 articles about 1-methyl 4-trichloroethyl itaconate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 2-methylene-4-oxo-4-(2,2,2-trichloroethoxy)butanoic acid

: 102651-57-0
1-methyl 4-trichloroethyl itaconate

Guidance literature:: DOI:10.1021/jo00366a023

Reference yield:

: 2170-03-8
itaconic acid anhydride

: 102651-57-0
1-methyl 4-trichloroethyl itaconate

Guidance literature:: Multi-step reaction with 2 steps

1: 34 percent / BF₃*2Et₂O / 0.5 h / 95 °C

2: 43 percent

With boron trifluoride dietherate;
DOI:10.1021/jo00366a023

Reference yield:

: 102651-57-0
1-methyl 4-trichloroethyl itaconate

: 102651-51-4
1-methyl 4-vinyl itaconate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / Zn, aq.HCl / ethanol / 0.33 h / 0 °C

2: LiCl*PdCl₂ / 31 h / Heating

With hydrogenchloride; lithium trichloropalladate; zinc; In ethanol;
DOI:10.1021/jo00366a023