(camphorquinone monooximato)bis(2-(3-methylphenylazo)pyridine)osmium(II) perchlorate monohydrate

Base Information

Chemical Name:(camphorquinone monooximato)bis(2-(3-methylphenylazo)pyridine)osmium(II) perchlorate monohydrate
CAS No.:442124-07-4
Molecular Formula:C₃₄H₃₆N₇O₂Os*ClO₄*H₂O
Molecular Weight:882.371
Hs Code.:

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Chemical Property of (camphorquinone monooximato)bis(2-(3-methylphenylazo)pyridine)osmium(II) perchlorate monohydrate

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Technology Process of (camphorquinone monooximato)bis(2-(3-methylphenylazo)pyridine)osmium(II) perchlorate monohydrate

There total 2 articles about (camphorquinone monooximato)bis(2-(3-methylphenylazo)pyridine)osmium(II) perchlorate monohydrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: cis-[OsCl(NO)(2-(3-methylphenylazo)pyridine)2]

: 736109-58-3,787517-91-3,68546-28-1
1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one

: sodium perchlorate

: 442124-07-4
(camphorquinone monooximato)bis(2-(3-methylphenylazo)pyridine)osmium(II) perchlorate monohydrate

Guidance literature:: With NaOCH₃; In methanol; water; to soln. of Os complex in MeOH added camphor, NaOMe; mixt. boiled under reflux for 1 h; filtered; solvent slowly evapd. in air; satd. aq. soln. of NaClO4 added; filtered; washed (H2O, Et2O); dried (vac. over P4O10); monitored by IR; elem. anal.;

Reference yield: 62.0%

: cis-dichloro-bis(2-(3-methylphenylazo)pyridine)osmium(II)

: sodium perchlorate

: 663-17-2
camphorquinone monooxime

: 442124-07-4
(camphorquinone monooximato)bis(2-(3-methylphenylazo)pyridine)osmium(II) perchlorate monohydrate

Guidance literature:: With CaCO₃; In 2-methoxy-ethanol; water; camphorquinone monooxime and CaCO3 added to suspn. of Os complex in MeOCH2CH2OH/H2O; mixt. boiled under reflux for 4 h; satd. aq. soln. of NaClO4 added; filtered; filtrate concd. by evapn. (vac.); residue washed (Et2O); dried(vac. over P4O10); redissolved (CH2Cl2); chromd. on silica gel; red ban d eluted (C6H6-MeCN); eluate slowly evapd.; crystals dried (vac., over P4O10); elem. anal.;